(R)-3-[1,3]Dithiolan-2-yl-3-(4-methoxy-phenyl)-5-(2-methyl-[1,3]dithiolan-2-yl)-pentan-1-ol

Base Information

Chemical Name:(R)-3-[1,3]Dithiolan-2-yl-3-(4-methoxy-phenyl)-5-(2-methyl-[1,3]dithiolan-2-yl)-pentan-1-ol
CAS No.:122172-30-9
Molecular Formula:C₁₉H₂₈O₂S₄
Molecular Weight:416.694
Hs Code.:

Synonyms:(R)-3-[1,3]Dithiolan-2-yl-3-(4-methoxy-phenyl)-5-(2-methyl-[1,3]dithiolan-2-yl)-pentan-1-ol

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Chemical Property of (R)-3-[1,3]Dithiolan-2-yl-3-(4-methoxy-phenyl)-5-(2-methyl-[1,3]dithiolan-2-yl)-pentan-1-ol

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Technology Process of (R)-3-[1,3]Dithiolan-2-yl-3-(4-methoxy-phenyl)-5-(2-methyl-[1,3]dithiolan-2-yl)-pentan-1-ol

There total 6 articles about (R)-3-[1,3]Dithiolan-2-yl-3-(4-methoxy-phenyl)-5-(2-methyl-[1,3]dithiolan-2-yl)-pentan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 122172-29-6
(R)-3-(4-methoxyphenyl)-3-<2-(1,3-dithiolanyl)>-5-<2-(2-methyl-1,3-dithiolanyl)>pentan-1-al

: 122172-30-9
(R)-3-[1,3]Dithiolan-2-yl-3-(4-methoxy-phenyl)-5-(2-methyl-[1,3]dithiolan-2-yl)-pentan-1-ol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.0833333h;
DOI:10.1021/jo00277a017

Reference yield:

: 122172-27-4
(S)-2-(4-methoxyphenyl)-2-<2-(1,3-dithiolanyl)>-4-<2-(2-methyl-1,3-dithiolanyl)>butanal

: 122172-30-9
(R)-3-[1,3]Dithiolan-2-yl-3-(4-methoxy-phenyl)-5-(2-methyl-[1,3]dithiolan-2-yl)-pentan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) phenyllithium / 1.) ether, 0 deg C, 2.) 0 deg C, 1 h

2: 1.) 10percent HCl, 2.) concd HCl / diethyl ether / 15 h

3: 89 percent / NaBH₄ / methanol / 0.08 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; phenyllithium; In methanol; diethyl ether;
DOI:10.1021/jo00277a017

Reference yield:

: 122172-26-3
(S)-2-(4-methoxyphenyl)-2-<2-(1,3-dithiolanyl)>-4-<2-(2-methyl-1,3-dithiolanyl)>butan-1-ol

: 122172-30-9
(R)-3-[1,3]Dithiolan-2-yl-3-(4-methoxy-phenyl)-5-(2-methyl-[1,3]dithiolan-2-yl)-pentan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 68 percent / pyridinium dichromate, sodium acetate / CH₂Cl₂ / 6 h / 0 °C

2: 1.) phenyllithium / 1.) ether, 0 deg C, 2.) 0 deg C, 1 h

3: 1.) 10percent HCl, 2.) concd HCl / diethyl ether / 15 h

4: 89 percent / NaBH₄ / methanol / 0.08 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; dipyridinium dichromate; sodium acetate; phenyllithium; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jo00277a017