Technology Process of C46H62N4O4
There total 19 articles about C46H62N4O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: cyclohexene / 10percent Pd/C / ethanol / 6.5 h / Heating
2: 90 percent / glacial acetic acid / 1 h / 80 °C
3: KOH/H2O / propan-1-ol / 3 h / Heating
4: DMF / 3 h / Heating
With
potassium hydroxide; water; acetic acid; N,N-dimethyl-formamide; cyclohexene;
palladium on activated charcoal;
In
propan-1-ol; ethanol;
DOI:10.1021/jo00233a011
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 86.2 percent / toluene / 19.5 h / Heating
2: K2CO3 / dioxane / 44 h / Heating
3: cyclohexene / 10percent Pd/C / ethanol / 6.5 h / Heating
4: 90 percent / glacial acetic acid / 1 h / 80 °C
5: KOH/H2O / propan-1-ol / 3 h / Heating
6: DMF / 3 h / Heating
With
potassium hydroxide; water; potassium carbonate; acetic acid; N,N-dimethyl-formamide; cyclohexene;
palladium on activated charcoal;
In
1,4-dioxane; propan-1-ol; ethanol; toluene;
DOI:10.1021/jo00233a011
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 43.4 percent / HI / ethanol / 1 h
2: 86.2 percent / toluene / 19.5 h / Heating
3: K2CO3 / dioxane / 44 h / Heating
4: cyclohexene / 10percent Pd/C / ethanol / 6.5 h / Heating
5: 90 percent / glacial acetic acid / 1 h / 80 °C
6: KOH/H2O / propan-1-ol / 3 h / Heating
7: DMF / 3 h / Heating
With
potassium hydroxide; water; hydrogen iodide; potassium carbonate; acetic acid; N,N-dimethyl-formamide; cyclohexene;
palladium on activated charcoal;
In
1,4-dioxane; propan-1-ol; ethanol; toluene;
DOI:10.1021/jo00233a011
