2,3-bis-(3,4-didodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-formyl phenyl ester

Base Information

Chemical Name:2,3-bis-(3,4-didodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-formyl phenyl ester
CAS No.:1262970-34-2
Molecular Formula:C₇₆H₁₁₄N₂O₇
Molecular Weight:1167.75
Hs Code.:

Synonyms:2,3-bis-(3,4-didodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-formyl phenyl ester

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Chemical Property of 2,3-bis-(3,4-didodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-formyl phenyl ester

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Technology Process of 2,3-bis-(3,4-didodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-formyl phenyl ester

There total 3 articles about 2,3-bis-(3,4-didodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-formyl phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1262970-33-1
2,3-bis(3,4-bis(dodecyloxy)phenyl)quinoxaline-6-carboxylic acid

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1262970-34-2
2,3-bis-(3,4-didodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-formyl phenyl ester

Guidance literature:: 2,3-bis(3,4-bis(dodecyloxy)phenyl)quinoxaline-6-carboxylic acid; 4-hydroxy-benzaldehyde; With dmap; In chloroform; for 0.5h; Inert atmosphere; Cooling with ice;

With dicyclohexyl-carbodiimide; In chloroform; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2010.11.014

Reference yield:

: 42244-53-1
1,2-bisdodecyloxybenzene

: 1262970-34-2
2,3-bis-(3,4-didodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-formyl phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: carbon disulfide; aluminum (III) chloride / 8 h / 0 °C / Inert atmosphere

2.1: acetic acid / tetrahydrofuran; ethanol / 12 h / Inert atmosphere; Reflux

3.1: dmap / chloroform / 0.5 h / Inert atmosphere; Cooling with ice

3.2: 12 h / 20 °C / Inert atmosphere

With carbon disulfide; dmap; aluminum (III) chloride; acetic acid; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1016/j.tet.2010.11.014

Reference yield:

: 138145-30-9
1,2-bis(3,4-bis(docosyloxy)phenyl)ethane-1,2-dione

: 1262970-34-2
2,3-bis-(3,4-didodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-formyl phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / tetrahydrofuran; ethanol / 12 h / Inert atmosphere; Reflux

2.1: dmap / chloroform / 0.5 h / Inert atmosphere; Cooling with ice

2.2: 12 h / 20 °C / Inert atmosphere

With dmap; acetic acid; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1016/j.tet.2010.11.014