4,6-di-O-tert-butyldiphenylsilyl-1,5-anhydro-2-deoxy-D-threo-hex-1-en-3-ulose

Base Information

Chemical Name:4,6-di-O-tert-butyldiphenylsilyl-1,5-anhydro-2-deoxy-D-threo-hex-1-en-3-ulose
CAS No.:1075749-04-0
Molecular Formula:C₃₈H₄₄O₄Si₂
Molecular Weight:620.936
Hs Code.:

Synonyms:4,6-di-O-tert-butyldiphenylsilyl-1,5-anhydro-2-deoxy-D-threo-hex-1-en-3-ulose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,6-di-O-tert-butyldiphenylsilyl-1,5-anhydro-2-deoxy-D-threo-hex-1-en-3-ulose

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Technology Process of 4,6-di-O-tert-butyldiphenylsilyl-1,5-anhydro-2-deoxy-D-threo-hex-1-en-3-ulose

There total 1 articles about 4,6-di-O-tert-butyldiphenylsilyl-1,5-anhydro-2-deoxy-D-threo-hex-1-en-3-ulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 14125-64-5,26242-05-7,105660-75-1
1,5-anhydro-2-deoxy-D-threo-hex-1-en-3-ulose

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1075749-04-0
4,6-di-O-tert-butyldiphenylsilyl-1,5-anhydro-2-deoxy-D-threo-hex-1-en-3-ulose

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1021/jo801596q

Reference yield: 82.0%

: 1075749-04-0
4,6-di-O-tert-butyldiphenylsilyl-1,5-anhydro-2-deoxy-D-threo-hex-1-en-3-ulose

: 1075749-12-0
C₃₈H₄₆O₄Si₂

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride heptahydrate; In methanol; at 0 ℃; for 4h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo801596q