3-(benzyloxy)-2,5-bis(benzoylamino)-6-(2,3-dihydroxypropyl)benzonitrile

Base Information

Chemical Name:3-(benzyloxy)-2,5-bis(benzoylamino)-6-(2,3-dihydroxypropyl)benzonitrile
CAS No.:174873-43-9
Molecular Formula:C₃₁H₂₇N₃O₅
Molecular Weight:521.572
Hs Code.:

Synonyms:3-(benzyloxy)-2,5-bis(benzoylamino)-6-(2,3-dihydroxypropyl)benzonitrile

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Chemical Property of 3-(benzyloxy)-2,5-bis(benzoylamino)-6-(2,3-dihydroxypropyl)benzonitrile

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Technology Process of 3-(benzyloxy)-2,5-bis(benzoylamino)-6-(2,3-dihydroxypropyl)benzonitrile

There total 12 articles about 3-(benzyloxy)-2,5-bis(benzoylamino)-6-(2,3-dihydroxypropyl)benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 174873-23-5
6-allyl-3-(benzyloxy)-2,5-bis(benzoylamino)benzonitrile

: 174873-43-9
3-(benzyloxy)-2,5-bis(benzoylamino)-6-(2,3-dihydroxypropyl)benzonitrile

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; at 25 ℃; for 12h;
DOI:10.1021/ja953777e

Reference yield: 58.0%

: C₄₃H₅₅N₃O₅Si₂

: 174873-43-9
3-(benzyloxy)-2,5-bis(benzoylamino)-6-(2,3-dihydroxypropyl)benzonitrile

: C₃₇H₄₁N₃O₅Si

Guidance literature:: With acetic acid; In tetrahydrofuran; water; at 25 ℃; for 48h;
DOI:10.1021/ja962431g

Reference yield:

: 25945-96-4
2-benzyloxy-4-nitro-phenylamine

: 174873-43-9
3-(benzyloxy)-2,5-bis(benzoylamino)-6-(2,3-dihydroxypropyl)benzonitrile

Guidance literature:: Multi-step reaction with 7 steps

1.1: 100 percent / NBS

2.1: 95 percent

3.1: 100 percent / Al-Hg

4.1: 96 percent

5.1: 84 percent / Pb(OAc)4 / 4 h / 25 °C

6.1: BF₃*Et₂O / CH₂Cl₂ / 0.5 h / -20 °C

6.2: 89 percent / CH₂Cl₂ / 3 h / -20 °C

7.1: 95 percent / N-methylmorpholine N-oxide / OsO₄ / acetone; H₂O; toluene / 25 °C

With lead(IV) acetate; N-Bromosuccinimide; aluminium amalgam; boron trifluoride diethyl etherate; 4-methylmorpholine N-oxide; osmium(VIII) oxide; In dichloromethane; water; acetone; toluene; 1.1: Bromination / 2.1: Substitution / 3.1: Reduction / 4.1: Acylation / 5.1: Oxidation / 6.1: Addition / 6.2: Addition / 7.1: hydroxylation;
DOI:10.1021/ja962431g