(S)-adamantan-1-yl 1-oxo-2-(2-(2-(trifluoromethyl)phenylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxylate

Base Information

Chemical Name:(S)-adamantan-1-yl 1-oxo-2-(2-(2-(trifluoromethyl)phenylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxylate
CAS No.:1041024-85-4
Molecular Formula:C₂₉H₃₀F₃NO₅S
Molecular Weight:561.622
Hs Code.:

Synonyms:(S)-adamantan-1-yl 1-oxo-2-(2-(2-(trifluoromethyl)phenylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxylate

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Chemical Property of (S)-adamantan-1-yl 1-oxo-2-(2-(2-(trifluoromethyl)phenylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxylate

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Technology Process of (S)-adamantan-1-yl 1-oxo-2-(2-(2-(trifluoromethyl)phenylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxylate

There total 2 articles about (S)-adamantan-1-yl 1-oxo-2-(2-(2-(trifluoromethyl)phenylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1039756-00-7
N-{[2-(trifluoromethyl)benzene]sulfonyl}aziridine

: 1-oxo-indan-2-carboxylic acid adamantan-1-yl ester

: 1041024-85-4
(S)-adamantan-1-yl 1-oxo-2-(2-(2-(trifluoromethyl)phenylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxylate

Guidance literature:: With dipotassium hydrogenphosphate; C₄₅H₄₇N₂O₂⁽¹⁺⁾*Cl^(1-); In chloroform; water; toluene; at -20 ℃; Reagent/catalyst; Temperature; enantioselective reaction; Catalytic behavior; Inert atmosphere;
DOI:10.1002/chem.201203825

Reference yield:

: 776-04-5
2-trifluoromethylbenzenesulfonyl chloride

: 1041024-85-4
(S)-adamantan-1-yl 1-oxo-2-(2-(2-(trifluoromethyl)phenylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0 °C / Inert atmosphere

1.2: 4 h / Inert atmosphere

2.1: C₄₅H₄₇N₂O₂⁽¹⁺⁾*Cl^(1-); dipotassium hydrogenphosphate / chloroform; water; toluene / -20 °C / Inert atmosphere

With dipotassium hydrogenphosphate; C₄₅H₄₇N₂O₂⁽¹⁺⁾*Cl^(1-); triethylamine; In dichloromethane; chloroform; water; toluene;
DOI:10.1002/chem.201203825