2-(3,4-difluorophenyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

Base Information

Chemical Name:2-(3,4-difluorophenyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one
CAS No.:1456613-89-0
Molecular Formula:C₁₀H₅F₂N₅OS
Molecular Weight:281.245
Hs Code.:

Synonyms:2-(3,4-difluorophenyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

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Chemical Property of 2-(3,4-difluorophenyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

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Technology Process of 2-(3,4-difluorophenyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

There total 5 articles about 2-(3,4-difluorophenyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1456614-11-1
C₁₂H₁₁F₂N₅O₂S

: 1456613-89-0
2-(3,4-difluorophenyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

Guidance literature:: With sodium hydroxide; In ethanol; water; at 100 ℃; for 0.333333h;
DOI:10.1016/j.ejmech.2013.06.051

Reference yield:

: C₈H₈F₂N₄O

: 1456613-89-0
2-(3,4-difluorophenyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: water / 180 °C / Microwave irradiation

2: N,N-dimethyl-formamide / 5 h / 20 °C

3: sodium hydroxide / ethanol; water / 0.33 h / 100 °C

With sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.06.051

Reference yield:

: 1016715-11-9
C₈H₆F₂N₄

: 1456613-89-0
2-(3,4-difluorophenyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 5 h / 20 °C

2: sodium hydroxide / ethanol; water / 0.33 h / 100 °C

With sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.06.051