(9H-fluoren-9-yl)methyl (S)-1-formamido-6-(benzyloxycarbonylamino)hexan-2-ylcarbamate

Base Information

Chemical Name:(9H-fluoren-9-yl)methyl (S)-1-formamido-6-(benzyloxycarbonylamino)hexan-2-ylcarbamate
CAS No.:1095037-81-2
Molecular Formula:C₃₀H₃₃N₃O₅
Molecular Weight:515.609
Hs Code.:

Synonyms:(9H-fluoren-9-yl)methyl (S)-1-formamido-6-(benzyloxycarbonylamino)hexan-2-ylcarbamate

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Chemical Property of (9H-fluoren-9-yl)methyl (S)-1-formamido-6-(benzyloxycarbonylamino)hexan-2-ylcarbamate

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Technology Process of (9H-fluoren-9-yl)methyl (S)-1-formamido-6-(benzyloxycarbonylamino)hexan-2-ylcarbamate

There total 3 articles about (9H-fluoren-9-yl)methyl (S)-1-formamido-6-(benzyloxycarbonylamino)hexan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₃₁N₃O₅

: 1095037-81-2
(9H-fluoren-9-yl)methyl (S)-1-formamido-6-(benzyloxycarbonylamino)hexan-2-ylcarbamate

Guidance literature:: With dmap; formic acid; In dichloromethane; at -15 ℃;
DOI:10.1021/jo801527d

Reference yield:

: 1095037-53-8
Fmoc-Lys(Z)-OH

: 1095037-81-2
(9H-fluoren-9-yl)methyl (S)-1-formamido-6-(benzyloxycarbonylamino)hexan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 4-methyl-morpholine

2: toluene / 65 °C

3: dmap; formic acid / dichloromethane / -15 °C

With 4-methyl-morpholine; dmap; formic acid; In dichloromethane; toluene;
DOI:10.1016/j.tetlet.2011.08.090

Reference yield:

: C₃₀H₃₁N₅O₅

: 1095037-81-2
(9H-fluoren-9-yl)methyl (S)-1-formamido-6-(benzyloxycarbonylamino)hexan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 65 °C

2: dmap; formic acid / dichloromethane / -15 °C

With dmap; formic acid; In dichloromethane; toluene;
DOI:10.1016/j.tetlet.2011.08.090