(S)-2-benzyloxycarbonyl-3-(N-phenylpiperazin-4-ylcarbonyl)-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:(S)-2-benzyloxycarbonyl-3-(N-phenylpiperazin-4-ylcarbonyl)-1,2,3,4-tetrahydroisoquinoline
CAS No.:473799-46-1
Molecular Formula:C₂₈H₂₉N₃O₃
Molecular Weight:455.557
Hs Code.:

Synonyms:(S)-2-benzyloxycarbonyl-3-(N-phenylpiperazin-4-ylcarbonyl)-1,2,3,4-tetrahydroisoquinoline

Suppliers and Price of (S)-2-benzyloxycarbonyl-3-(N-phenylpiperazin-4-ylcarbonyl)-1,2,3,4-tetrahydroisoquinoline

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Chemical Property of (S)-2-benzyloxycarbonyl-3-(N-phenylpiperazin-4-ylcarbonyl)-1,2,3,4-tetrahydroisoquinoline

Chemical Property:

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Technology Process of (S)-2-benzyloxycarbonyl-3-(N-phenylpiperazin-4-ylcarbonyl)-1,2,3,4-tetrahydroisoquinoline

There total 1 articles about (S)-2-benzyloxycarbonyl-3-(N-phenylpiperazin-4-ylcarbonyl)-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79261-58-8
(S)-3,4-dihydro-1H-isoquinoline-2,3-dicarboxylic acid 2-benzyl ester

: 473799-46-1
(S)-2-benzyloxycarbonyl-3-(N-phenylpiperazin-4-ylcarbonyl)-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: DCC / dimethylformamide / 4 h / 70 °C

2: dimethylformamide / 17 h / 20 °C

With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

Reference yield: 70.0%

: 473799-46-1
(S)-2-benzyloxycarbonyl-3-(N-phenylpiperazin-4-ylcarbonyl)-1,2,3,4-tetrahydroisoquinoline

: 473799-47-2
(S)-3-(N-phenylpiperazin-4-ylcarbonyl)-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With hydrogen bromide; In acetic acid; at 0 - 20 ℃; for 10h;

Reference yield:

: 473799-46-1
(S)-2-benzyloxycarbonyl-3-(N-phenylpiperazin-4-ylcarbonyl)-1,2,3,4-tetrahydroisoquinoline

: (S)-3-(N-phenylpiperazin-4-ylcarbonyl)-2-(1-naphthalenesulfonyloxy)-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / HBr / acetic acid / 10 h / 0 - 20 °C

2: 89 percent / EtN₃ / dioxane / 12 h / 20 °C

With hydrogen bromide; ethyl azide; In 1,4-dioxane; acetic acid;