2-(3,5-di-(p-chlorophenyl)isoxazol-4-ylsulfonylmethyl)-4,5-dihydro-oxazole

Base Information

Chemical Name:2-(3,5-di-(p-chlorophenyl)isoxazol-4-ylsulfonylmethyl)-4,5-dihydro-oxazole
CAS No.:1339152-74-7
Molecular Formula:C₁₉H₁₄Cl₂N₂O₄S
Molecular Weight:437.303
Hs Code.:

Synonyms:2-(3,5-di-(p-chlorophenyl)isoxazol-4-ylsulfonylmethyl)-4,5-dihydro-oxazole

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Chemical Property of 2-(3,5-di-(p-chlorophenyl)isoxazol-4-ylsulfonylmethyl)-4,5-dihydro-oxazole

Chemical Property:

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Technology Process of 2-(3,5-di-(p-chlorophenyl)isoxazol-4-ylsulfonylmethyl)-4,5-dihydro-oxazole

There total 3 articles about 2-(3,5-di-(p-chlorophenyl)isoxazol-4-ylsulfonylmethyl)-4,5-dihydro-oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1339152-37-2
2-(4,5-dihydro-3,5-di-(4-chlorophenyl)isoxazol-4-ylsulfonylmethyl)-4,5-dihydrooxazole

: 1339152-74-7
2-(3,5-di-(p-chlorophenyl)isoxazol-4-ylsulfonylmethyl)-4,5-dihydro-oxazole

Guidance literature:: With chloranil; In 5,5-dimethyl-1,3-cyclohexadiene; Reflux;
DOI:10.1016/j.ejmech.2011.08.010

Reference yield:

: 1038996-88-1
C₁₁H₁₁ClO₄S

: 1339152-74-7
2-(3,5-di-(p-chlorophenyl)isoxazol-4-ylsulfonylmethyl)-4,5-dihydro-oxazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: samarium(III) chloride; n-butyllithium / toluene / 0.33 h / 0 °C

1.2: Reflux

2.1: chloroamine-T / methanol / Reflux

3.1: chloranil / 5,5-dimethyl-1,3-cyclohexadiene / Reflux

With n-butyllithium; samarium(III) chloride; chloroamine-T; chloranil; In methanol; 5,5-dimethyl-1,3-cyclohexadiene; toluene;
DOI:10.1016/j.ejmech.2011.08.010

Reference yield:

: 1339152-87-2
2-(2-(p-chlorophenyl)ethenesulfonylmethyl)-4,5-dihydrooxazole

: 1339152-74-7
2-(3,5-di-(p-chlorophenyl)isoxazol-4-ylsulfonylmethyl)-4,5-dihydro-oxazole

Guidance literature:: Multi-step reaction with 2 steps

1: chloroamine-T / methanol / Reflux

2: chloranil / 5,5-dimethyl-1,3-cyclohexadiene / Reflux

With chloroamine-T; chloranil; In methanol; 5,5-dimethyl-1,3-cyclohexadiene;
DOI:10.1016/j.ejmech.2011.08.010