H₃V₁₀O₂₈^(3-)*3P(C₆H₅)4⁽¹⁺⁾=H₃V₁₀O₂₈{(C₆H₅)4P}3

Base Information

• Chemical Name: H₃V₁₀O₂₈^(3-)*3P(C₆H₅)4⁽¹⁺⁾=H₃V₁₀O₂₈{(C₆H₅)4P}3
• CAS No.: 55261-63-7
• Molecular Formula: 3C₂₄H₂₀P*H₃O₂₈V₁₀
• Molecular Weight: 1978.61
• Mol file: 55261-63-7.mol

Synonyms:H₃V₁₀O₂₈^(3-)*3P(C₆H₅)4⁽¹⁺⁾=H₃V₁₀O₂₈{(C₆H₅)4P}3

Chemical Property of H₃V₁₀O₂₈^(3-)*3P(C₆H₅)4⁽¹⁺⁾=H₃V₁₀O₂₈{(C₆H₅)4P}3

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of H₃V₁₀O₂₈^(3-)*3P(C₆H₅)4⁽¹⁺⁾=H₃V₁₀O₂₈{(C₆H₅)4P}3

There total 1 articles about H₃V₁₀O₂₈^(3-)*3P(C₆H₅)4⁽¹⁺⁾=H₃V₁₀O₂₈{(C₆H₅)4P}3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

Sodium orthovanadate + tetraphenylphosphonium bromide (2751-90-8) → H3V10O28(3-)*3P(C6H5)4(1+)=H3V10O28{(C6H5)4P}3 (55261-63-7)

Guidance literature:

With HCl; In water; dropwise addn. of HCl to a stirred soln. of Na3VO4 in deionized H2O until the formed ppt. was redissolved; addn. of the orange soln. in portions to a stirred soln. of (C6H5)4PBr in deionized H2O; stirring for 5-10 min;; ppt.; suction filtration; washed with H2O, ethanol, and ether; dried in vac. for 3 h; stirring of the crude material in dry CH3CN for 10 min; gravity filtration; ether was slowly poured into the filtrate; crystn. on standing for 15 min; elem. anal.;;

DOI:10.1021/ja00244a022

upstream raw materials:

tetraphenylphosphonium bromide