ALPHA-HOMONOJIRIMYCIN

Base Information

• Chemical Name: ALPHA-HOMONOJIRIMYCIN
• CAS No.: 119557-99-2
• Molecular Formula: C₇H₁₅NO₅
• Molecular Weight: 193.2
• Mol file: 119557-99-2.mol

Synonyms:3,4,5-Piperidinetriol,2,6-bis(hydroxymethyl)-, [2R-(2a,3a,4b,5a,6b)]- (9CI); 2,6-Dideoxy-2,6-imino-D-glycero-L-gulo-heptitol;Homonojirimycin; a-Homonojirimycin

Chemical Property of ALPHA-HOMONOJIRIMYCIN

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 207 °C
• Refractive Index: 84.5 ° (C=1, H2O)
• Boiling Point: 432°Cat760mmHg
• Flash Point: 224.7°C
• PSA: 113.18000
• Density: 1.479g/cm³
• LogP: -3.27710
• Storage Temp.: Freezer

Purity/Quality:

98%,99%, ^*data from raw suppliers

a-Homonojirimycin ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: α-Homonojirimycin (HMJ) is used as an inhibitor of several carbohydrate degrading enzymes including α-glucosidases, glycoprotein processing enzyme glucosidase II and maltase.

Technology Process of ALPHA-HOMONOJIRIMYCIN

There total 38 articles about ALPHA-HOMONOJIRIMYCIN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

7-O-tert-butyldimethylsilyl-2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-D-glycero-D-talo-heptitol (127903-43-9) → α-homomannojirimycin (76215-89-9,119557-99-2,127995-31-7,127995-29-3)

Guidance literature:

With trifluoroacetic acid; In water;

DOI:10.1016/S0040-4039(01)93952-8

Reference yield: 86.0%

C22H27NO6 → α-homomannojirimycin (76215-89-9,119557-99-2,127995-31-7,127995-29-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1016/j.bmcl.2018.03.035

Reference yield: 85.0%

7-O-tert-butyldimethylsilyl-2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-L-glycero-D-talo-heptitol (127995-32-8) → β-homoaltronojirimycin (76215-89-9,119557-99-2,127995-29-3,127995-31-7)

Guidance literature:

With trifluoroacetic acid;

DOI:10.1016/S0040-4039(01)93952-8

upstream raw materials:

(3aS,4R,6R,7R,7aS)-4-(tert-Butyl-dimethyl-silanyloxymethyl)-7-methoxymethoxy-6-methoxymethoxymethyl-2,2-dimethyl-hexahydro-[1,3]dioxolo[4,5-c]pyridine

2,6-dideoxy-2,6-imino-D-glycero-L-gulo-heptitol 1,3,4,5-tetrabenzoate

Methanesulfonic acid (S)-1-[(4R,5S)-5-((1R,2R)-2-amino-1,3-bis-methoxymethoxy-propyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-2-(tert-butyl-dimethyl-silanyloxy)-ethyl ester

Benzyl-[(1R,2R)-2-((4R,5S)-2,2-dimethyl-5-vinyl-[1,3]dioxolan-4-yl)-2-methoxymethoxy-1-methoxymethoxymethyl-ethyl]-carbamic acid benzyl ester

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