S-benzyl N,N-dibenzyl-4-methoxyphenylphosphonamidodithioate

Base Information

• Chemical Name: S-benzyl N,N-dibenzyl-4-methoxyphenylphosphonamidodithioate
• CAS No.: 78906-71-5
• Molecular Formula: C₂₈H₂₈NOPS₂
• Molecular Weight: 489.642
• Mol file: 78906-71-5.mol

Synonyms:S-benzyl N,N-dibenzyl-4-methoxyphenylphosphonamidodithioate

Chemical Property of S-benzyl N,N-dibenzyl-4-methoxyphenylphosphonamidodithioate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of S-benzyl N,N-dibenzyl-4-methoxyphenylphosphonamidodithioate

There total 2 articles about S-benzyl N,N-dibenzyl-4-methoxyphenylphosphonamidodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Lawessons reagent (19172-47-5,94367-93-8) + dibenzylamine (103-49-1) → tribenzylamine (620-40-6) + S-benzyl N-benzyl-4-methoxyphenylphosphonamidodithioate (78906-72-6) + S,S-dibenzyl 4-methoxyphenylphosphonotrithioate (78906-73-7) + S-benzyl N,N-dibenzyl-4-methoxyphenylphosphonamidodithioate (78906-71-5)

Guidance literature:

In xylene; at 230 ℃; for 18h; Further byproducts given. Title compound not separated from byproducts; Heating; other temp.;

DOI:10.1016/S0040-4020(01)97679-3

Reference yield:

Lawessons reagent (19172-47-5,94367-93-8) + dibenzylamine (103-49-1) → S-benzyl N-benzyl-4-methoxyphenylphosphonamidodithioate (78906-72-6) + S,S-dibenzyl 4-methoxyphenylphosphonotrithioate (78906-73-7) + N,N,N'-tribenzyl-4-methoxyphenylphosphonothioic diamide (78906-70-4) + S-benzyl N,N-dibenzyl-4-methoxyphenylphosphonamidodithioate (78906-71-5)

Guidance literature:

In xylene; at 140 ℃; for 18h; Further byproducts given; Heating; other temp.;

DOI:10.1016/S0040-4020(01)97679-3

upstream raw materials:

Lawessons reagent

dibenzylamine