[PdCl(P(C₆H₁₁)2CH₂C(C(CH₃)3)NNC(C(CH₃)3)CH₂P(C₆H₁₁)2)]⁽¹⁺⁾*Cl^(1-)=[PdCl(P(C₆H₁₁)2CH₂C(C₄H₉)NNC(C₄H₉)CH₂P(C₆H₁₁)2)]Cl

Base Information

• Chemical Name: [PdCl(P(C₆H₁₁)2CH₂C(C(CH₃)3)NNC(C(CH₃)3)CH₂P(C₆H₁₁)2)]⁽¹⁺⁾*Cl^(1-)=[PdCl(P(C₆H₁₁)2CH₂C(C₄H₉)NNC(C₄H₉)CH₂P(C₆H₁₁)2)]Cl
• CAS No.: 819870-25-2
• Molecular Formula: C₃₆H₆₆ClN₂P₂Pd*Cl
• Molecular Weight: 766.207

Synonyms:[PdCl(P(C₆H₁₁)2CH₂C(C(CH₃)3)NNC(C(CH₃)3)CH₂P(C₆H₁₁)2)]⁽¹⁺⁾*Cl^(1-)=[PdCl(P(C₆H₁₁)2CH₂C(C₄H₉)NNC(C₄H₉)CH₂P(C₆H₁₁)2)]Cl

Chemical Property of [PdCl(P(C₆H₁₁)2CH₂C(C(CH₃)3)NNC(C(CH₃)3)CH₂P(C₆H₁₁)2)]⁽¹⁺⁾*Cl^(1-)=[PdCl(P(C₆H₁₁)2CH₂C(C₄H₉)NNC(C₄H₉)CH₂P(C₆H₁₁)2)]Cl

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Technology Process of [PdCl(P(C₆H₁₁)2CH₂C(C(CH₃)3)NNC(C(CH₃)3)CH₂P(C₆H₁₁)2)]⁽¹⁺⁾*Cl^(1-)=[PdCl(P(C₆H₁₁)2CH₂C(C₄H₉)NNC(C₄H₉)CH₂P(C₆H₁₁)2)]Cl

There total 2 articles about [PdCl(P(C₆H₁₁)2CH₂C(C(CH₃)3)NNC(C(CH₃)3)CH₂P(C₆H₁₁)2)]⁽¹⁺⁾*Cl^(1-)=[PdCl(P(C₆H₁₁)2CH₂C(C₄H₉)NNC(C₄H₉)CH₂P(C₆H₁₁)2)]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

dichloro bis(acetonitrile) palladium(II) (21264-30-2,90243-59-7,14592-56-4) + (C6H11)2PCH2C(C(CH3)3)NNC(C(CH3)3)CH2P(C6H11)2 → [PdCl(P(C6H11)2CH2C(C(CH3)3)NNC(C(CH3)3)CH2P(C6H11)2)](1+)*Cl(1-)=[PdCl(P(C6H11)2CH2C(C4H9)NNC(C4H9)CH2P(C6H11)2)]Cl (819870-25-2)

Guidance literature:

In chloroform; (Ar); standard Schlenk technique; soln. of azine diphosphine in CHCl3 was added to soln. of Pd complex in CHCl3; mixt. was stirred under reflux for 2 h; cooled to ambient temp.; filtered; concd.; heptane added; kept for 1 d; filtered; dried (vac.);

DOI:10.1016/j.ica.2004.06.022

Reference yield:

bis(benzonitrile)palladium(II) dichloride (15617-18-2,39958-10-6,14220-64-5) + (C6H11)2PCH2C(C(CH3)3)NNC(C(CH3)3)CH2P(C6H11)2 → [PdCl2(P(C6H11)2CH2C(C(CH3)3)NNC(C(CH3)3)CH2P(C6H11)2)] + [PdCl(P(C6H11)2CH2C(C(CH3)3)NNC(C(CH3)3)CH2P(C6H11)2)](1+)*Cl(1-)=[PdCl(P(C6H11)2CH2C(C4H9)NNC(C4H9)CH2P(C6H11)2)]Cl (819870-25-2)

Guidance literature:

In chloroform; (Ar); standard Schlenk technique; azine diphosphine (1 equiv.) and Pd complex (1 equiv.) were reacted in CHCl3 at room temp.;

DOI:10.1016/j.ica.2004.06.022

Reference yield: 71.0%

[PdCl(P(C6H11)2CH2C(C(CH3)3)NNC(C(CH3)3)CH2P(C6H11)2)](1+)*Cl(1-)=[PdCl(P(C6H11)2CH2C(C4H9)NNC(C4H9)CH2P(C6H11)2)]Cl (819870-25-2) → [(C(t-Bu)CHP(c-C6H11)2)N(NC(t-Bu)CH2P(c-C6H11)2)PdCl] (819870-28-5)

Guidance literature:

With Et₃N; In dichloromethane; (Ar); standard Schlenk technique; Et3N (8 equiv.) was added to soln. of Pd complex in CH2Cl2; mixt. was stirred at room temp. for 20 min; evapd.; extd. (hexane); evapd.; dried (vac.);

DOI:10.1016/j.ica.2004.06.022

upstream raw materials:

dichloro bis(acetonitrile) palladium(II)

bis(benzonitrile)palladium(II) dichloride

Downstream raw materials:

[(C(t-Bu)CHP(c-C₆H₁₁)2)N(NC(t-Bu)CH₂P(c-C₆H₁₁)2)PdCl]

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