Tetrakis(4-methoxyphenyl)ethylene

Base Information

• Chemical Name: Tetrakis(4-methoxyphenyl)ethylene
• CAS No.: 10019-24-6
• Molecular Formula: C30H28 O4
• Molecular Weight: 452.55
• Hs Code.: 2909309090
• NSC Number: 132124
• DSSTox Substance ID: DTXSID00142999
• Nikkaji Number: J2.291H
• Wikidata: Q83006637
• Mol file: 10019-24-6.mol

Synonyms:tetrakis(4-methoxyphenyl)ethylene;tetrakis(p-methoxyphenyl)ethylene

Chemical Property of Tetrakis(4-methoxyphenyl)ethylene

Chemical Property:

• Melting Point: 183 °C
• Boiling Point: 574.1±45.0 °C(Predicted)
• Flash Point: 123.1oC
• PSA: 36.92000
• Density: 1.126±0.06 g/cm3(Predicted)
• LogP: 6.72840
• XLogP3: 7.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 8
• Exact Mass: 452.19875937
• Heavy Atom Count: 34
• Complexity: 508

Purity/Quality:

≥99% ^*data from raw suppliers

1,1,2,2-Tetrakis(4-methoxyphenyl)ethene 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)C(=C(C2=CC=C(C=C2)OC)C3=CC=C(C=C3)OC)C4=CC=C(C=C4)OC

Technology Process of Tetrakis(4-methoxyphenyl)ethylene

There total 54 articles about Tetrakis(4-methoxyphenyl)ethylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

triphenylphosphorane (153785-57-0) → 1,1,2,2-tetrakis(4-methoxyphenyl)ethene (10019-24-6)

Guidance literature:

With woollins’ reagent; In toluene; for 1h; Heating;

DOI:10.1039/b702818k

Reference yield: 99.0%

bis(p-methoxyphenyl)methanone (90-96-0) → 1,1,2,2-tetrakis(4-methoxyphenyl)ethene (10019-24-6)

Guidance literature:

With woollins’ reagent; In toluene; for 20h; Heating;

DOI:10.1039/b702818k

Reference yield: 98.0%

1,1,2,2-tetrakis(4-methoxyphenyl)ethene (10019-24-6) → tetraanisylethylene cation-radical (10019-24-6)

Guidance literature:

With methanesulfonic acid; chloranil; In dichloromethane; at 25 ℃; for 0.333333h;

DOI:10.3891/acta.chem.scand.52-0114

upstream raw materials:

thioformaldehyde

Bis(p-methoxyphenyl)diazomethan

dichloro-bis-(4-methoxy-phenyl)-methane

2-acetoxy-1,1,1,2-tetrakis-(4-methoxy-phenyl)-ethane

Downstream raw materials:

1,1,2,2-tetrakis(4-methoxyphenyl)ethane

tetra(p-hydroxyphenyl)ethylene

1,2-dichloro-1,1,2,2-tetrakis-(3,5-dichloro-4-methoxy-phenyl)-ethane

tetrakis-(4-methoxy-phenyl)-oxirane