Methyl 2-hydroxy-6-tridecylbenzoate

Base Information

• Chemical Name: Methyl 2-hydroxy-6-tridecylbenzoate
• CAS No.: 75808-38-7
• Molecular Formula: C₂₁H₃₄O₃
• Molecular Weight: 334.499
• Mol file: 75808-38-7.mol

Synonyms:Methyl 2-hydroxy-6-tridecylbenzoate

Chemical Property of Methyl 2-hydroxy-6-tridecylbenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Methyl 2-hydroxy-6-tridecylbenzoate

There total 4 articles about Methyl 2-hydroxy-6-tridecylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

methyl 2-methoxy-6-tridecyl benzoate (100485-96-9) → Methyl 2-hydroxy-6-tridecylbenzoate (75808-38-7)

Guidance literature:

With aluminium(III) iodide; In carbon disulfide; Heating;

Reference yield:

Methyl 2-hexadecynoate (63125-05-3) → Methyl 2-hydroxy-6-tridecylbenzoate (75808-38-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / dichloromaleic anhydride / 200 °C

2: 77 percent / AlI₃ / CS₂ / Heating

With aluminium(III) iodide; dichloromaleic acid anhydride; In carbon disulfide;

Reference yield:

Methyl 3-oxo-2-(triphenylphosphoranylidene)hexadecanoate (63125-03-1) → Methyl 2-hydroxy-6-tridecylbenzoate (75808-38-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 58 percent / 1.5 h / 260 - 263 °C / 0.02 Torr

2: 75 percent / dichloromaleic anhydride / 200 °C

3: 77 percent / AlI₃ / CS₂ / Heating

With aluminium(III) iodide; dichloromaleic acid anhydride; In carbon disulfide;

upstream raw materials:

diazomethane

2-hydroxy-6-tridecylbenzoic acid

methyl 2-methoxy-6-tridecyl benzoate

Methyl 2-hexadecynoate

Downstream raw materials:

2-hydroxy-6-tridecylbenzoic acid