(2S,3S,6S)-1-Dibenzylamino-6-((S)-1-hydroxy-propyl)-2-((R)-1-phenyl-ethylcarbamoyl)-1,2,3,6-tetrahydro-pyridine-3-sulfinic acid

Base Information

Chemical Name:(2S,3S,6S)-1-Dibenzylamino-6-((S)-1-hydroxy-propyl)-2-((R)-1-phenyl-ethylcarbamoyl)-1,2,3,6-tetrahydro-pyridine-3-sulfinic acid
CAS No.:1027279-83-9
Molecular Formula:C₃₁H₃₇N₃O₄S
Molecular Weight:547.718
Hs Code.:

Synonyms:(2S,3S,6S)-1-Dibenzylamino-6-((S)-1-hydroxy-propyl)-2-((R)-1-phenyl-ethylcarbamoyl)-1,2,3,6-tetrahydro-pyridine-3-sulfinic acid

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Chemical Property of (2S,3S,6S)-1-Dibenzylamino-6-((S)-1-hydroxy-propyl)-2-((R)-1-phenyl-ethylcarbamoyl)-1,2,3,6-tetrahydro-pyridine-3-sulfinic acid

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Technology Process of (2S,3S,6S)-1-Dibenzylamino-6-((S)-1-hydroxy-propyl)-2-((R)-1-phenyl-ethylcarbamoyl)-1,2,3,6-tetrahydro-pyridine-3-sulfinic acid

There total 3 articles about (2S,3S,6S)-1-Dibenzylamino-6-((S)-1-hydroxy-propyl)-2-((R)-1-phenyl-ethylcarbamoyl)-1,2,3,6-tetrahydro-pyridine-3-sulfinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 816453-04-0
(1R,3aS,5S,7aS)-4-Dibenzylamino-5-((S)-1-hydroxy-propyl)-1-oxo-2-((R)-1-phenyl-ethyl)-1,2,3a,4,5,7a-hexahydro-1λ⁴-isothiazolo[4,5-b]pyridin-3-one

: 1027279-83-9
(2S,3S,6S)-1-Dibenzylamino-6-((S)-1-hydroxy-propyl)-2-((R)-1-phenyl-ethylcarbamoyl)-1,2,3,6-tetrahydro-pyridine-3-sulfinic acid

Guidance literature:: With sodium hydroxide; In water; acetone; at 0 - 20 ℃; for 6.5h;
DOI:10.1021/jo048581o

Reference yield:

: 2-((R)-1-Phenyl-ethyl)-isothiazol-3-one

: 1027279-83-9
(2S,3S,6S)-1-Dibenzylamino-6-((S)-1-hydroxy-propyl)-2-((R)-1-phenyl-ethylcarbamoyl)-1,2,3,6-tetrahydro-pyridine-3-sulfinic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: 3.8 g / m-chloroperoxybenzoic acid / CH₂Cl₂ / 3 h / 0 °C

2.1: toluene / 70 h / 85 °C

2.2: 62 percent / NaHCO₃ / H₂O; toluene / 0.5 h / 20 °C

3.1: NaOH / acetone; H₂O / 6.5 h / 0 - 20 °C

With sodium hydroxide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; acetone; toluene;
DOI:10.1021/jo048581o

Reference yield:

: 700380-06-9
(R)-1-Oxo-2-((R)-1-phenyl-ethyl)-1,2-dihydro-1λ⁴-isothiazol-3-one

: 1027279-83-9
(2S,3S,6S)-1-Dibenzylamino-6-((S)-1-hydroxy-propyl)-2-((R)-1-phenyl-ethylcarbamoyl)-1,2,3,6-tetrahydro-pyridine-3-sulfinic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 70 h / 85 °C

1.2: 62 percent / NaHCO₃ / H₂O; toluene / 0.5 h / 20 °C

2.1: NaOH / acetone; H₂O / 6.5 h / 0 - 20 °C

With sodium hydroxide; In water; acetone; toluene;
DOI:10.1021/jo048581o