N,N-dimethyl-3-(3-(2-(phenylethynyl)phenyl)-1-(trimethylsilyl)propa-1,2-dienyl)aniline

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Chemical Name:N,N-dimethyl-3-(3-(2-(phenylethynyl)phenyl)-1-(trimethylsilyl)propa-1,2-dienyl)aniline
CAS No.:1575770-50-1
Molecular Formula:C₂₉H₂₉N
Molecular Weight:391.556
Hs Code.:

Synonyms:N,N-dimethyl-3-(3-(2-(phenylethynyl)phenyl)-1-(trimethylsilyl)propa-1,2-dienyl)aniline

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Chemical Property of N,N-dimethyl-3-(3-(2-(phenylethynyl)phenyl)-1-(trimethylsilyl)propa-1,2-dienyl)aniline

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Technology Process of N,N-dimethyl-3-(3-(2-(phenylethynyl)phenyl)-1-(trimethylsilyl)propa-1,2-dienyl)aniline

There total 1 articles about N,N-dimethyl-3-(3-(2-(phenylethynyl)phenyl)-1-(trimethylsilyl)propa-1,2-dienyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 4,4-dimethyl-1-(2-(phenylethynyl)phenyl)pent-2-ynyl acetate

: 86967-66-0
(3-(dimethylamino)phenyl)magnesium bromide

: 1575770-50-1
N,N-dimethyl-3-(3-(2-(phenylethynyl)phenyl)-1-(trimethylsilyl)propa-1,2-dienyl)aniline

Guidance literature:: (3-(dimethylamino)phenyl)magnesium bromide; With zinc(II) chloride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 0.5h; Inert atmosphere;

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; at -60 ℃; for 0.25h; Inert atmosphere;

4,4-dimethyl-1-(2-(phenylethynyl)phenyl)pent-2-ynyl acetate; In tetrahydrofuran; diethyl ether; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo500035b