2,5-Dibutoxy-8,11-diphenyl-8,11-dihydro-3,4,7,8,9,10,11,12-octaaza-dicyclopenta[c,g]phenathrene

Base Information

• Chemical Name: 2,5-Dibutoxy-8,11-diphenyl-8,11-dihydro-3,4,7,8,9,10,11,12-octaaza-dicyclopenta[c,g]phenathrene
• CAS No.: 120401-86-7
• Molecular Formula: C₃₂H₃₀N₈O₂
• Molecular Weight: 558.643
• Mol file: 120401-86-7.mol

Synonyms:2,5-Dibutoxy-8,11-diphenyl-8,11-dihydro-3,4,7,8,9,10,11,12-octaaza-dicyclopenta[c,g]phenathrene

Chemical Property of 2,5-Dibutoxy-8,11-diphenyl-8,11-dihydro-3,4,7,8,9,10,11,12-octaaza-dicyclopenta[c,g]phenathrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-Dibutoxy-8,11-diphenyl-8,11-dihydro-3,4,7,8,9,10,11,12-octaaza-dicyclopenta[c,g]phenathrene

There total 5 articles about 2,5-Dibutoxy-8,11-diphenyl-8,11-dihydro-3,4,7,8,9,10,11,12-octaaza-dicyclopenta[c,g]phenathrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

6,6'-Dibutoxy-2,2'-diphenyl-2H,2'H-[4,4']bibenzotriazolyl-5,5'-diamine (120401-88-9) → 2,5-Dibutoxy-8,11-diphenyl-8,11-dihydro-3,4,7,8,9,10,11,12-octaaza-dicyclopenta[c,g]phenathrene (120401-86-7)

Guidance literature:

With oxygen; copper(l) chloride; In pyridine; at 60 ℃;

DOI:10.1007/BF00961933

Reference yield:

5-amino-6-butoxy-2-phenylbenzotriazole (82811-24-3) → 2,5-Dibutoxy-8,11-diphenyl-8,11-dihydro-3,4,7,8,9,10,11,12-octaaza-dicyclopenta[c,g]phenathrene (120401-86-7) + 5,11-Dibutoxy-2,8-diphenyl-2,8-dihydro-1,2,3,6,7,8,9,12-octaaza-dicyclopenta[a,h]anthracene (120401-87-8)

Guidance literature:

With oxygen; copper(l) chloride; In pyridine; at 60 ℃; Title compound not separated from byproducts;

DOI:10.1007/BF00961933

Reference yield:

5-amino-6-butoxy-2-phenylbenzotriazole (82811-24-3) → 2,5-Dibutoxy-8,11-diphenyl-8,11-dihydro-3,4,7,8,9,10,11,12-octaaza-dicyclopenta[c,g]phenathrene (120401-86-7) + 5,11-Dibutoxy-2,8-diphenyl-2,8-dihydro-1,2,3,6,7,8,9,12-octaaza-dicyclopenta[a,h]anthracene (120401-87-8) + 6,6'-Dibutoxy-2,2'-diphenyl-2H,2'H-[4,4']bibenzotriazolyl-5,5'-diamine (120401-88-9)

Guidance literature:

With oxygen; copper(l) chloride; In pyridine; at 15 - 20 ℃; Title compound not separated from byproducts;

DOI:10.1007/BF00961933

upstream raw materials:

2,4-diamino-5-butoxyazobenzene

5-amino-6-butoxy-2-phenylbenzotriazole

6,6'-Dibutoxy-2,2'-diphenyl-2H,2'H-[4,4']bibenzotriazolyl-5,5'-diamine