Technology Process of C25H27N5O3S
There total 8 articles about C25H27N5O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
for 2h;
Reflux;
- Guidance literature:
-
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
for 2h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C
2.1: potassium phosphate / tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide; water / 0.5 h / 100 °C
3.1: toluene; ethanol / 18 h / Molecular sieve; Reflux
3.2: 0.17 h / 0 °C
4.1: potassium carbonate / methanol / 2 h / 60 °C
5.1: hydrogenchloride / methanol / 2 h
6.1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / Reflux
With
hydrogenchloride; potassium phosphate; n-butyllithium; dimethylsulfide borane complex; potassium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; toluene;