C-phenyl 2,3:5,6-di-O-isopropylidene-α-d-talofuranoside

Base Information

Chemical Name:C-phenyl 2,3:5,6-di-O-isopropylidene-α-d-talofuranoside
CAS No.:1415308-13-2
Molecular Formula:C₁₈H₂₄O₅
Molecular Weight:320.386
Hs Code.:

Synonyms:C-phenyl 2,3:5,6-di-O-isopropylidene-α-d-talofuranoside

Suppliers and Price of C-phenyl 2,3:5,6-di-O-isopropylidene-α-d-talofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C-phenyl 2,3:5,6-di-O-isopropylidene-α-d-talofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C-phenyl 2,3:5,6-di-O-isopropylidene-α-d-talofuranoside

There total 2 articles about C-phenyl 2,3:5,6-di-O-isopropylidene-α-d-talofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1415325-89-1
(1S)-2,3:5,6-di-O-isopropylidene-1-C-phenyl-D-talitol

: 1415308-13-2
C-phenyl 2,3:5,6-di-O-isopropylidene-α-d-talofuranoside

: 1415308-17-6
C-phenyl 2,3:5,6-di-O-isopropylidene-β-d-talofuranoside

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; stereospecific reaction; Inert atmosphere; Reflux;
DOI:10.1016/j.carres.2012.08.023

Reference yield:

: 7306-64-1,14440-56-3,23262-80-8,27108-15-2,49561-21-9,67642-42-6
2,3,5,6-di-O-isopropylidene-D-mannono-1,4-lactone

: 1415308-13-2
C-phenyl 2,3:5,6-di-O-isopropylidene-α-d-talofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: piperidine / ethyl acetate / 5 h / 0 - 20 °C

1.2: 0 - 20 °C

2.1: dibutyl ether; tetrahydrofuran / 1 h / -78 °C

3.1: L-Selectride / tetrahydrofuran / -78 - 20 °C

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

With piperidine; di-isopropyl azodicarboxylate; L-Selectride; triphenylphosphine; In tetrahydrofuran; dibutyl ether; ethyl acetate;
DOI:10.1016/j.carres.2012.08.023