(benzyloxycarbonyl)-L-phenylalanyl-L-leucyl-L-lysinal hydrochloride

Base Information

Chemical Name:(benzyloxycarbonyl)-L-phenylalanyl-L-leucyl-L-lysinal hydrochloride
CAS No.:122314-37-8
Molecular Formula:C₂₉H₄₀N₄O₅*ClH
Molecular Weight:561.121
Hs Code.:

Synonyms:(benzyloxycarbonyl)-L-phenylalanyl-L-leucyl-L-lysinal hydrochloride

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Chemical Property of (benzyloxycarbonyl)-L-phenylalanyl-L-leucyl-L-lysinal hydrochloride

Chemical Property:

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Technology Process of (benzyloxycarbonyl)-L-phenylalanyl-L-leucyl-L-lysinal hydrochloride

There total 7 articles about (benzyloxycarbonyl)-L-phenylalanyl-L-leucyl-L-lysinal hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2389-49-3
N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-L-lysine methyl ester

: 122314-37-8
(benzyloxycarbonyl)-L-phenylalanyl-L-leucyl-L-lysinal hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: diisobutylaluminum hydride (DIBAL) / toluene; hexane / 3 h / -50 °C

2: sodium acetate / ethanol; H₂O / 0.75 h / Heating

3: 73 percent / H₂, 1 M hydrochloric acid / 10percent Pd/C / methanol / 3.5 h

4: triethylamine / CHCl₃ / 3 h / 0 °C

5: 1.) 37percent formalin, 0.1 M hydrochloric acid, 2.) 4 M hydrochloric acid / 1.) methanol, 0 deg C, 2 h, 2.) dioxane, 0 deg C, 3 h

With hydrogenchloride; formaldehyd; hydrogen; sodium acetate; diisobutylaluminium hydride; triethylamine; palladium on activated charcoal; In methanol; ethanol; hexane; chloroform; water; toluene;
DOI:10.1021/jm00163a014

Reference yield:

: 122314-13-0
tert-butyl-N-[(5S)-5-(benzyloxycarbonylamino)-6-oxo-hexyl]carbamate

: 122314-37-8
(benzyloxycarbonyl)-L-phenylalanyl-L-leucyl-L-lysinal hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: sodium acetate / ethanol; H₂O / 0.75 h / Heating

2: 73 percent / H₂, 1 M hydrochloric acid / 10percent Pd/C / methanol / 3.5 h

3: triethylamine / CHCl₃ / 3 h / 0 °C

4: 1.) 37percent formalin, 0.1 M hydrochloric acid, 2.) 4 M hydrochloric acid / 1.) methanol, 0 deg C, 2 h, 2.) dioxane, 0 deg C, 3 h

With hydrogenchloride; formaldehyd; hydrogen; sodium acetate; triethylamine; palladium on activated charcoal; In methanol; ethanol; chloroform; water;
DOI:10.1021/jm00163a014

Reference yield:

: 122314-18-5
N^α-(benzyloxycarbonyl)-N^ε-(tert-butoxycarbonyl)-L-lysinal semicarbazone

: 122314-37-8
(benzyloxycarbonyl)-L-phenylalanyl-L-leucyl-L-lysinal hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / H₂, 1 M hydrochloric acid / 10percent Pd/C / methanol / 3.5 h

2: triethylamine / CHCl₃ / 3 h / 0 °C

3: 1.) 37percent formalin, 0.1 M hydrochloric acid, 2.) 4 M hydrochloric acid / 1.) methanol, 0 deg C, 2 h, 2.) dioxane, 0 deg C, 3 h

With hydrogenchloride; formaldehyd; hydrogen; triethylamine; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1021/jm00163a014