[Cu(2-(pyridin-2-yl)-5-(p-tolyl)-1,3,4-oxadiazole)(PPh₃)₂]BF₄

Base Information

• Chemical Name: [Cu(2-(pyridin-2-yl)-5-(p-tolyl)-1,3,4-oxadiazole)(PPh₃)₂]BF₄
• CAS No.: 1245722-51-3
• Molecular Formula: BF₄*C₅₀H₄₁CuN₃OP₂
• Molecular Weight: 912.193
• Mol file: 1245722-51-3.mol

Synonyms:[Cu(2-(pyridin-2-yl)-5-(p-tolyl)-1,3,4-oxadiazole)(PPh₃)₂]BF₄

Chemical Property of [Cu(2-(pyridin-2-yl)-5-(p-tolyl)-1,3,4-oxadiazole)(PPh₃)₂]BF₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Cu(2-(pyridin-2-yl)-5-(p-tolyl)-1,3,4-oxadiazole)(PPh₃)₂]BF₄

There total 3 articles about [Cu(2-(pyridin-2-yl)-5-(p-tolyl)-1,3,4-oxadiazole)(PPh₃)₂]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

tetrakis(acetonitrile)copper(I)tetrafluoroborate + 2-(pyridyl-2-yl)-5-(p-tolyl)-1,3,4-oxadiazole (1171635-04-3) + triphenylphosphine (603-35-0) → [Cu(2-(pyridin-2-yl)-5-(p-tolyl)-1,3,4-oxadiazole)(PPh3)2]BF4 (1245722-51-3)

Guidance literature:

In dichloromethane; for 1h;

DOI:10.1016/j.ica.2013.02.020

Reference yield:

p-Toluic acid (99-94-5) → [Cu(2-(pyridin-2-yl)-5-(p-tolyl)-1,3,4-oxadiazole)(PPh3)2]BF4 (1245722-51-3)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride / 20 °C

2: pyridine / Reflux

3: dichloromethane / 1 h

With thionyl chloride; In pyridine; dichloromethane;

DOI:10.1016/j.ica.2013.02.020

Reference yield:

4-methyl-benzoyl chloride (874-60-2) → [Cu(2-(pyridin-2-yl)-5-(p-tolyl)-1,3,4-oxadiazole)(PPh3)2]BF4 (1245722-51-3)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / Reflux

2: dichloromethane / 1 h

In pyridine; dichloromethane;

DOI:10.1016/j.ica.2013.02.020

upstream raw materials:

2-(pyridyl-2-yl)-5-(p-tolyl)-1,3,4-oxadiazole

triphenylphosphine

p-Toluic acid

4-methyl-benzoyl chloride