1-(((4-(4-bromophenyl)-2-methylbut-3-yn-2-yl)oxy)methyl)-2-nitrobenzene

Base Information

Chemical Name:1-(((4-(4-bromophenyl)-2-methylbut-3-yn-2-yl)oxy)methyl)-2-nitrobenzene
CAS No.:1453814-02-2
Molecular Formula:C₁₈H₁₆BrNO₃
Molecular Weight:374.234
Hs Code.:

Synonyms:1-(((4-(4-bromophenyl)-2-methylbut-3-yn-2-yl)oxy)methyl)-2-nitrobenzene

Suppliers and Price of 1-(((4-(4-bromophenyl)-2-methylbut-3-yn-2-yl)oxy)methyl)-2-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(((4-(4-bromophenyl)-2-methylbut-3-yn-2-yl)oxy)methyl)-2-nitrobenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(((4-(4-bromophenyl)-2-methylbut-3-yn-2-yl)oxy)methyl)-2-nitrobenzene

There total 3 articles about 1-(((4-(4-bromophenyl)-2-methylbut-3-yn-2-yl)oxy)methyl)-2-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 612-25-9
2-Nitrobenzyl alcohol

: 76347-62-1
4-(3-hydroxy-3,3-dimethyl-1-propynyl)-1-bromobenzene

: 1453814-02-2
1-(((4-(4-bromophenyl)-2-methylbut-3-yn-2-yl)oxy)methyl)-2-nitrobenzene

Guidance literature:: With copper(ll) bromide; In nitromethane; at 20 ℃; for 12h; Darkness;
DOI:10.1016/j.tetlet.2013.07.144

Reference yield:

: 115-19-5
2-methyl-but-3-yn-2-ol

: 1453814-02-2
1-(((4-(4-bromophenyl)-2-methylbut-3-yn-2-yl)oxy)methyl)-2-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; copper(l) iodide; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 12 h / 75 °C / Inert atmosphere

2: copper(ll) bromide / nitromethane / 12 h / 20 °C / Darkness

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; copper(ll) bromide; In tetrahydrofuran; nitromethane; 1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.tetlet.2013.07.144

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 1453814-02-2
1-(((4-(4-bromophenyl)-2-methylbut-3-yn-2-yl)oxy)methyl)-2-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; copper(l) iodide; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 12 h / 75 °C / Inert atmosphere

2: copper(ll) bromide / nitromethane / 12 h / 20 °C / Darkness

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; copper(ll) bromide; In tetrahydrofuran; nitromethane; 1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.tetlet.2013.07.144