C₂₇H₂₈N₂O₅

Base Information

Chemical Name:C₂₇H₂₈N₂O₅
CAS No.:1408236-86-1
Molecular Formula:C₂₇H₂₈N₂O₅
Molecular Weight:460.53
Hs Code.:

C<sub>27</sub>H<sub>28</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₇H₂₈N₂O₅

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Chemical Property of C₂₇H₂₈N₂O₅

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Technology Process of C₂₇H₂₈N₂O₅

There total 8 articles about C₂₇H₂₈N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1408236-99-6
C₂₇H₂₈N₂O₅

: 1408236-86-1
C₂₇H₂₈N₂O₅

Guidance literature:: With sodium tetrachloroaurate(III) dihyrate; In ethanol; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol3027945

Reference yield:

: 1408236-94-1
C₂₁H₂₇NO₇

: 1408236-86-1
C₂₇H₂₈N₂O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: triethylamine / dichloromethane / 2 h / 0 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 20 h / 100 °C

3.1: potassium hydroxide / water; ethanol / 2 h / 120 °C

3.2: 4 h / 20 °C

4.1: dimethylsulfide borane complex / tetrahydrofuran / 12 h / 0 °C

5.1: iodine; potassium carbonate / methanol; water / 24 h / 20 °C

6.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 2 h / 90 °C

7.1: tri-n-butyl-tin hydride; Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

8.1: potassium carbonate / methanol / 2 h / 0 - 20 °C / Inert atmosphere

9.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(II) sulfate; sodium L-ascorbate / N,N-dimethyl-formamide / 5 h / 80 °C / Inert atmosphere

10.1: sodium tetrachloroaurate(III) dihyrate / ethanol / 4 h / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium tetrachloroaurate(III) dihyrate; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; iodine; tri-n-butyl-tin hydride; potassium carbonate; caesium carbonate; Dess-Martin periodane; copper(II) sulfate; sodium L-ascorbate; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene; 8.1: |Seyferth-Gilbert Homologation / 9.1: |Sonogashira Cross-Coupling;
DOI:10.1021/ol3027945

Reference yield:

: 1408236-88-3
C₂₁H₂₅NO₆

: 1408236-86-1
C₂₇H₂₈N₂O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium hydroxide / water; ethanol / 2 h / 120 °C

1.2: 4 h / 20 °C

2.1: dimethylsulfide borane complex / tetrahydrofuran / 12 h / 0 °C

3.1: iodine; potassium carbonate / methanol; water / 24 h / 20 °C

4.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 2 h / 90 °C

5.1: tri-n-butyl-tin hydride; Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

6.1: potassium carbonate / methanol / 2 h / 0 - 20 °C / Inert atmosphere

7.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(II) sulfate; sodium L-ascorbate / N,N-dimethyl-formamide / 5 h / 80 °C / Inert atmosphere

8.1: sodium tetrachloroaurate(III) dihyrate / ethanol / 4 h / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium tetrachloroaurate(III) dihyrate; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; iodine; tri-n-butyl-tin hydride; potassium carbonate; Dess-Martin periodane; copper(II) sulfate; sodium L-ascorbate; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene; 6.1: |Seyferth-Gilbert Homologation / 7.1: |Sonogashira Cross-Coupling;
DOI:10.1021/ol3027945