Technology Process of C62H86O6Si2
There total 4 articles about C62H86O6Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine;
In
ethyl acetate;
at 60 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1021/ma101816z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere; Darkness
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / ethyl acetate / 0.5 h / 60 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine;
In
tetrahydrofuran; ethyl acetate;
2: Sonogashira coupling;
DOI:10.1021/ma101816z
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
1.2: 40 °C / Inert atmosphere
2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / ethyl acetate / 0.25 h / 40 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere; Darkness
4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / ethyl acetate / 0.5 h / 60 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; sodium hydride; triethylamine;
In
tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide;
2.1: Sonogashira coupling / 4.1: Sonogashira coupling;
DOI:10.1021/ma101816z