14-bromo-13,13-bis(bromomethyl)-1,1,1-triphenyl-2,5,8,11-tetraoxatetradecane

Base Information

Chemical Name:14-bromo-13,13-bis(bromomethyl)-1,1,1-triphenyl-2,5,8,11-tetraoxatetradecane
CAS No.:1403503-23-0
Molecular Formula:C₃₀H₃₅Br₃O₄
Molecular Weight:699.317
Hs Code.:

Synonyms:14-bromo-13,13-bis(bromomethyl)-1,1,1-triphenyl-2,5,8,11-tetraoxatetradecane

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Chemical Property of 14-bromo-13,13-bis(bromomethyl)-1,1,1-triphenyl-2,5,8,11-tetraoxatetradecane

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Technology Process of 14-bromo-13,13-bis(bromomethyl)-1,1,1-triphenyl-2,5,8,11-tetraoxatetradecane

There total 2 articles about 14-bromo-13,13-bis(bromomethyl)-1,1,1-triphenyl-2,5,8,11-tetraoxatetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 3229-00-3
pentaerythritol tetrabromide

: 133699-09-9
10,10,10-triphenyl-3,6,9-trioxadecan-1-ol

: 1403503-23-0
14-bromo-13,13-bis(bromomethyl)-1,1,1-triphenyl-2,5,8,11-tetraoxatetradecane

Guidance literature:: 10,10,10-triphenyl-3,6,9-trioxadecan-1-ol; With sodium hydride; In diethylene glycol dimethyl ether; mineral oil; at 0 - 20 ℃; for 3h; Inert atmosphere;

pentaerythritol tetrabromide; In diethylene glycol dimethyl ether; mineral oil; at 165 ℃; Inert atmosphere;
DOI:10.1021/jo301718y

Reference yield:

: 76-83-5
trityl chloride

: 112-27-6
2,2'-[1,2-ethanediylbis(oxy)]bisethanol

: 1403503-23-0
14-bromo-13,13-bis(bromomethyl)-1,1,1-triphenyl-2,5,8,11-tetraoxatetradecane

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0 °C

2.1: sodium hydride / mineral oil; diethylene glycol dimethyl ether / 3 h / 0 - 20 °C / Inert atmosphere

2.2: 165 °C / Inert atmosphere

With sodium hydride; triethylamine; In dichloromethane; diethylene glycol dimethyl ether; mineral oil;
DOI:10.1021/jo301718y