C₃₈H₇₀O₆Si₃

Base Information

Chemical Name:C₃₈H₇₀O₆Si₃
CAS No.:1254331-95-7
Molecular Formula:C₃₈H₇₀O₆Si₃
Molecular Weight:707.227
Hs Code.:

C<sub>38</sub>H<sub>70</sub>O<sub>6</sub>Si<sub>3</sub>

Synonyms:C₃₈H₇₀O₆Si₃

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Chemical Property of C₃₈H₇₀O₆Si₃

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Technology Process of C₃₈H₇₀O₆Si₃

There total 7 articles about C₃₈H₇₀O₆Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1254331-85-5
(2S,4E,6S,8E,10S)-12-(4-methoxybenzyloxy)-2,6,10-tri(tert-butyldimethylsilyloxy)dodeca-4,8-dienenitrile

: 1254331-95-7
C₃₈H₇₀O₆Si₃

Guidance literature:: With diisobutylaluminium hydride; In n-heptane; toluene; at -78 - -10 ℃; for 9h;
DOI:10.1021/ol1021417

Reference yield:

: 1254331-93-5
(S)-4-(4-methoxybenzyloxy)-2-hydroxybutanenitrile

: 1254331-95-7
C₃₈H₇₀O₆Si₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / dichloromethane / 24 h / 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / toluene; n-heptane / 9 h / -78 - -10 °C / Inert atmosphere

3.1: tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

3.2: 3 h / -78 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / toluene; n-heptane / 9 h / -78 - -10 °C / Inert atmosphere

5.1: tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

5.2: 3 h / -78 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / toluene; n-heptane / 9 h / -78 - -10 °C / Inert atmosphere

With 1H-imidazole; diisobutylaluminium hydride; In tetrahydrofuran; n-heptane; dichloromethane; toluene; 3.1: |Julia-Kocienski Olefination / 3.2: |Julia-Kocienski Olefination / 5.1: |Julia-Kocienski Olefination / 5.2: |Julia-Kocienski Olefination;
DOI:10.1021/acs.joc.8b02034

Reference yield:

: 1254331-94-6
(S)-4-(4-methoxybenzyloxy)-2-(tert-butyldimethylsilyloxy)butanenitrile

: 1254331-95-7
C₃₈H₇₀O₆Si₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / toluene; n-heptane / 9 h / -78 - -10 °C / Inert atmosphere

2.1: tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

2.2: 3 h / -78 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / toluene; n-heptane / 9 h / -78 - -10 °C / Inert atmosphere

4.1: tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

4.2: 3 h / -78 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / toluene; n-heptane / 9 h / -78 - -10 °C / Inert atmosphere

With diisobutylaluminium hydride; In tetrahydrofuran; n-heptane; toluene; 2.1: |Julia-Kocienski Olefination / 2.2: |Julia-Kocienski Olefination / 4.1: |Julia-Kocienski Olefination / 4.2: |Julia-Kocienski Olefination;
DOI:10.1021/acs.joc.8b02034