(2R,4S,5R)-5-[(3E,7R,11Z,13R,14S,15E)-16-iodo-12-methoxycarbonyl-13-methoxymethoxy-4,7,14-trimethyl-5-oxo-6-oxahexadeca-3,11,15-trienyl]-4-[(1E,3E)-3-methyl-6-(trimethylsilyl)hexa-1,3-dien-5-ynyl]-2-phenyl-1,3-dioxane

Base Information

Chemical Name:(2R,4S,5R)-5-[(3E,7R,11Z,13R,14S,15E)-16-iodo-12-methoxycarbonyl-13-methoxymethoxy-4,7,14-trimethyl-5-oxo-6-oxahexadeca-3,11,15-trienyl]-4-[(1E,3E)-3-methyl-6-(trimethylsilyl)hexa-1,3-dien-5-ynyl]-2-phenyl-1,3-dioxane
CAS No.:1000211-07-3
Molecular Formula:C₄₂H₅₉IO₈Si
Molecular Weight:846.916
Hs Code.:

(2R,4S,5R)-5-[(3E,7R,11Z,13R,14S,15E)-16-iodo-12-methoxycarbonyl-13-methoxymethoxy-4,7,14-trimethyl-5-oxo-6-oxahexadeca-3,11,15-trienyl]-4-[(1E,3E)-3-methyl-6-(trimethylsilyl)hexa-1,3-dien-5-ynyl]-2-phenyl-1,3-dioxane

Synonyms:(2R,4S,5R)-5-[(3E,7R,11Z,13R,14S,15E)-16-iodo-12-methoxycarbonyl-13-methoxymethoxy-4,7,14-trimethyl-5-oxo-6-oxahexadeca-3,11,15-trienyl]-4-[(1E,3E)-3-methyl-6-(trimethylsilyl)hexa-1,3-dien-5-ynyl]-2-phenyl-1,3-dioxane

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Chemical Property of (2R,4S,5R)-5-[(3E,7R,11Z,13R,14S,15E)-16-iodo-12-methoxycarbonyl-13-methoxymethoxy-4,7,14-trimethyl-5-oxo-6-oxahexadeca-3,11,15-trienyl]-4-[(1E,3E)-3-methyl-6-(trimethylsilyl)hexa-1,3-dien-5-ynyl]-2-phenyl-1,3-dioxane

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Technology Process of (2R,4S,5R)-5-[(3E,7R,11Z,13R,14S,15E)-16-iodo-12-methoxycarbonyl-13-methoxymethoxy-4,7,14-trimethyl-5-oxo-6-oxahexadeca-3,11,15-trienyl]-4-[(1E,3E)-3-methyl-6-(trimethylsilyl)hexa-1,3-dien-5-ynyl]-2-phenyl-1,3-dioxane

There total 1 articles about (2R,4S,5R)-5-[(3E,7R,11Z,13R,14S,15E)-16-iodo-12-methoxycarbonyl-13-methoxymethoxy-4,7,14-trimethyl-5-oxo-6-oxahexadeca-3,11,15-trienyl]-4-[(1E,3E)-3-methyl-6-(trimethylsilyl)hexa-1,3-dien-5-ynyl]-2-phenyl-1,3-dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1000211-03-9
(1E,3S,4R,5Z,10R)-10-[(2RS)-2-(diethoxyphosphonoyl)propionyloxy]-1-iodo-5-methoxycarbonyl-4-methoxymethoxy-3-methylundeca-1,5-diene

: C₂₃H₃₀O₃Si

: 1000211-07-3
(2R,4S,5R)-5-[(3E,7R,11Z,13R,14S,15E)-16-iodo-12-methoxycarbonyl-13-methoxymethoxy-4,7,14-trimethyl-5-oxo-6-oxahexadeca-3,11,15-trienyl]-4-[(1E,3E)-3-methyl-6-(trimethylsilyl)hexa-1,3-dien-5-ynyl]-2-phenyl-1,3-dioxane

Guidance literature:: (1E,3S,4R,5Z,10R)-10-[(2RS)-2-(diethoxyphosphonoyl)propionyloxy]-1-iodo-5-methoxycarbonyl-4-methoxymethoxy-3-methylundeca-1,5-diene; With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile; at 0 ℃; for 0.5h;

C₂₃H₃₀O₃Si; In acetonitrile; at 0 ℃; for 1h; Further stages.;
DOI:10.1016/j.tetlet.2007.10.002