((Z)-N-(3,5-bis(4-(tert-butyl)phenyl)-2H-pyrrol-2-ylidene)-3,5-bis(4-(tert-butyl)phenyl)-1H-pyrrol-2-amine)

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Chemical Name:((Z)-N-(3,5-bis(4-(tert-butyl)phenyl)-2H-pyrrol-2-ylidene)-3,5-bis(4-(tert-butyl)phenyl)-1H-pyrrol-2-amine)
CAS No.:1334171-77-5
Molecular Formula:C₄₈H₅₅N₃
Molecular Weight:673.985
Hs Code.:

Synonyms:((Z)-N-(3,5-bis(4-(tert-butyl)phenyl)-2H-pyrrol-2-ylidene)-3,5-bis(4-(tert-butyl)phenyl)-1H-pyrrol-2-amine)

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Chemical Property of ((Z)-N-(3,5-bis(4-(tert-butyl)phenyl)-2H-pyrrol-2-ylidene)-3,5-bis(4-(tert-butyl)phenyl)-1H-pyrrol-2-amine)

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Technology Process of ((Z)-N-(3,5-bis(4-(tert-butyl)phenyl)-2H-pyrrol-2-ylidene)-3,5-bis(4-(tert-butyl)phenyl)-1H-pyrrol-2-amine)

There total 4 articles about ((Z)-N-(3,5-bis(4-(tert-butyl)phenyl)-2H-pyrrol-2-ylidene)-3,5-bis(4-(tert-butyl)phenyl)-1H-pyrrol-2-amine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1334171-91-3
1,3-bis(4-(tert-butyl)phenyl)-4-nitrobutan-1-one

: 1334171-77-5
((Z)-N-(3,5-bis(4-(tert-butyl)phenyl)-2H-pyrrol-2-ylidene)-3,5-bis(4-(tert-butyl)phenyl)-1H-pyrrol-2-amine)

Guidance literature:: With ammonium acetate; In butan-1-ol; for 24h; Reflux;
DOI:10.1021/ol202211t

Reference yield:

: 1334171-90-2
(E)-1,3-bis(4-(tert-butyl)phenyl)prop-2-en-1-one

: 1334171-77-5
((Z)-N-(3,5-bis(4-(tert-butyl)phenyl)-2H-pyrrol-2-ylidene)-3,5-bis(4-(tert-butyl)phenyl)-1H-pyrrol-2-amine)

Guidance literature:: Multi-step reaction with 2 steps

1: diethylamine / methanol / 24 h / Reflux

2: ammonium acetate / butan-1-ol / 24 h / Reflux

With ammonium acetate; diethylamine; In methanol; butan-1-ol;
DOI:10.1021/ol202211t

Reference yield:

: 939-97-9
4-tert-Butylbenzaldehyde

: 1334171-77-5
((Z)-N-(3,5-bis(4-(tert-butyl)phenyl)-2H-pyrrol-2-ylidene)-3,5-bis(4-(tert-butyl)phenyl)-1H-pyrrol-2-amine)

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol; water / 20 °C

2: diethylamine / methanol / 24 h / Reflux

3: ammonium acetate / butan-1-ol / 24 h / Reflux

With ammonium acetate; diethylamine; potassium hydroxide; In methanol; ethanol; water; butan-1-ol;
DOI:10.1021/ol202211t