3-[6-(benzyloxycarbonamido)-2-methyl-7,8-dihydro-1-naphthyl]propanoic acid

Base Information

Chemical Name:3-[6-(benzyloxycarbonamido)-2-methyl-7,8-dihydro-1-naphthyl]propanoic acid
CAS No.:253784-75-7
Molecular Formula:C₂₂H₂₃NO₄
Molecular Weight:365.429
Hs Code.:

Synonyms:3-[6-(benzyloxycarbonamido)-2-methyl-7,8-dihydro-1-naphthyl]propanoic acid

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Chemical Property of 3-[6-(benzyloxycarbonamido)-2-methyl-7,8-dihydro-1-naphthyl]propanoic acid

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Technology Process of 3-[6-(benzyloxycarbonamido)-2-methyl-7,8-dihydro-1-naphthyl]propanoic acid

There total 1 articles about 3-[6-(benzyloxycarbonamido)-2-methyl-7,8-dihydro-1-naphthyl]propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 621-84-1
O-benzyl carbamate

: 253784-71-3
3-(2-methyl-6-oxo-5,6,7,8-tetrahydronaphtalen-1-yl)propanoic acid

: 253784-75-7
3-[6-(benzyloxycarbonamido)-2-methyl-7,8-dihydro-1-naphthyl]propanoic acid

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 20h; Heating;
DOI:10.1016/S0957-4166(99)00375-4

Reference yield: 95.0%

: 253784-75-7
3-[6-(benzyloxycarbonamido)-2-methyl-7,8-dihydro-1-naphthyl]propanoic acid

: 253784-91-7
3-(6-benzyloxycarbonylamino-2-methyl-5,6,7,8-tetrahydro-naphthalen-1-yl)-propionic acid

Guidance literature:: With ((R)-(1,1'-binaphthyl-2,2'-diyl)bis(diphenylphosphine))Ru(O₂CCF₃)2; hydrogen; In methanol; at 50 ℃; for 60h; under 75006 Torr;
DOI:10.1016/S0957-4166(99)00375-4

Reference yield:

: 253784-75-7
3-[6-(benzyloxycarbonamido)-2-methyl-7,8-dihydro-1-naphthyl]propanoic acid

: 3-[6-(benzyloxycarbonamido)-2-methyl-5,6,7,8-tetrahydro-1-naphthyl]propanoic acid

Guidance literature:: With hydrogen; ((R)-(1,1'-binaphthyl-2,2'-diyl)bis(diphenylphosphine))Ru(O₂CCF₃)2; In methanol; at 50 ℃; for 60h; under 75006 Torr; Title compound not separated from byproducts;
DOI:10.1135/cccc20020235