C₂₉H₄₂O₃Si

Base Information

Chemical Name:C₂₉H₄₂O₃Si
CAS No.:949148-98-5
Molecular Formula:C₂₉H₄₂O₃Si
Molecular Weight:466.736
Hs Code.:

C<sub>29</sub>H<sub>42</sub>O<sub>3</sub>Si

Synonyms:C₂₉H₄₂O₃Si

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Chemical Property of C₂₉H₄₂O₃Si

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Technology Process of C₂₉H₄₂O₃Si

There total 9 articles about C₂₉H₄₂O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 949148-89-4
(2S,6S,7R,8S,E)-8-(tert-butyldiphenylsilyloxy)-7-methoxy-2,4,6-trimethylnon-4-en-1-ol

: 949148-98-5
C₂₉H₄₂O₃Si

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane;
DOI:10.1021/ol701427k

Reference yield:

: 949148-84-9
(E)-(S)-3-(dimethyl-phenyl-silanyl)-3-methyl-hex-4-enoic acid methyl ester

: 949148-98-5
C₂₉H₄₂O₃Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 62 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 24 h / -50 °C

2.1: LiOH / tetrahydrofuran; methanol; H₂O / 3 h / 20 °C

3.1: oxalyl chloride / CH₂Cl₂; dimethylformamide / 20 °C

4.1: 1.68 g / diethyl ether / 0.5 h / 0 °C

5.1: 80 percent / silver benzoate / CH₂Cl₂ / 0.08 h / 20 °C

6.1: lithium diisopropylamide / tetrahydrofuran; hexane / 1.75 h / -78 - 0 °C

6.2: tetrahydrofuran; hexane / 0.5 h / 0 °C

7.1: lithium diisopropylamide; BH₃*NH₃ / tetrahydrofuran; hexane / 2 h / 20 °C

8.1: 100 percent / oxalyl chloride; methyl sulfoxide; triethylamine / CH₂Cl₂

With lithium hydroxide; borane-ammonia complex; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; silver benzoate; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide; 8.1: Swern oxidation;
DOI:10.1021/ol701427k

Reference yield:

: (2S,6S,7R,8S,E)-8-(tert-butyldiphenylsilyloxy)-N-((1S,2S)-1-hydroxy-1-phenylpropan-2-yl)-7-methoxy-N,2,4,6-tetramethylnon-4-enamide

: 949148-98-5
C₂₉H₄₂O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: lithium diisopropylamide; BH₃*NH₃ / tetrahydrofuran; hexane / 2 h / 20 °C

2: 100 percent / oxalyl chloride; methyl sulfoxide; triethylamine / CH₂Cl₂

With borane-ammonia complex; oxalyl dichloride; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; 2: Swern oxidation;
DOI:10.1021/ol701427k