trans,trans-(S)-(-)-2-(N-methyl-N-cinnamoylamino)-3-phenylpropyl cinnamoate

Base Information

Chemical Name:trans,trans-(S)-(-)-2-(N-methyl-N-cinnamoylamino)-3-phenylpropyl cinnamoate
CAS No.:157059-69-3
Molecular Formula:C₂₈H₂₇NO₃
Molecular Weight:425.527
Hs Code.:

Synonyms:trans,trans-(S)-(-)-2-(N-methyl-N-cinnamoylamino)-3-phenylpropyl cinnamoate

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Chemical Property of trans,trans-(S)-(-)-2-(N-methyl-N-cinnamoylamino)-3-phenylpropyl cinnamoate

Chemical Property:

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Technology Process of trans,trans-(S)-(-)-2-(N-methyl-N-cinnamoylamino)-3-phenylpropyl cinnamoate

There total 3 articles about trans,trans-(S)-(-)-2-(N-methyl-N-cinnamoylamino)-3-phenylpropyl cinnamoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 84773-29-5
(S)-(+)-2-(N-methylamino)-3-phenylpropanol

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 157059-69-3
trans,trans-(S)-(-)-2-(N-methyl-N-cinnamoylamino)-3-phenylpropyl cinnamoate

Guidance literature:: With triethylamine; In tetrachloromethane; 0 deg C, 30 min; 25 deg C, 6 h;
DOI:10.1016/S0040-4020(01)80705-5

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 157059-69-3
trans,trans-(S)-(-)-2-(N-methyl-N-cinnamoylamino)-3-phenylpropyl cinnamoate

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / acetic anhydride / 0 deg C, 10 min; rt, 4 h

2: 90 percent / LiAlH₄ / tetrahydrofuran / 0 deg C, 30 min, rt, 3 h; reflux, 9 h

3: 90 percent / Et₃N / CCl₄ / 0 deg C, 30 min; 25 deg C, 6 h

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; tetrachloromethane; acetic anhydride;
DOI:10.1016/S0040-4020(01)80705-5

Reference yield:

: 13200-85-6
N-formyl-L-phenylalanine

: 157059-69-3
trans,trans-(S)-(-)-2-(N-methyl-N-cinnamoylamino)-3-phenylpropyl cinnamoate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / LiAlH₄ / tetrahydrofuran / 0 deg C, 30 min, rt, 3 h; reflux, 9 h

2: 90 percent / Et₃N / CCl₄ / 0 deg C, 30 min; 25 deg C, 6 h

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; tetrachloromethane;
DOI:10.1016/S0040-4020(01)80705-5