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C20H24O4

Base Information
  • Chemical Name:C20H24O4
  • CAS No.:1449419-23-1
  • Molecular Formula:C20H24O4
  • Molecular Weight:328.408
  • Hs Code.:
C<sub>20</sub>H<sub>24</sub>O<sub>4</sub>

Synonyms:C20H24O4

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Chemical Property of C20H24O4
Chemical Property:
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Technology Process of C20H24O4

There total 6 articles about C20H24O4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium hydrogencarbonate; methyl iodide; In water; acetonitrile; at 20 ℃; for 19h;
DOI:10.1016/j.tet.2013.02.008
Guidance literature:
Multi-step reaction with 6 steps
1.1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 °C
1.2: 2.5 h / 0 - 20 °C
2.1: magnesium bromide ethyl etherate / dichloromethane / 1 h / -78 °C
2.2: 1.5 h / -78 °C
3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran; toluene / 21 h / 0 - 20 °C
4.1: sodium hydroxide / tetrahydrofuran; water; methanol / 12 h / 0 - 20 °C
5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C
5.2: 21.5 h / 0 - 20 °C
6.1: sodium hydrogencarbonate; methyl iodide / acetonitrile; water / 19 h / 20 °C
With di-isopropyl azodicarboxylate; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; magnesium bromide ethyl etherate; triphenylphosphine; sodium hydroxide; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile; mineral oil; 2.2: |Grignard Reaction / 3.1: |Mitsunobu Displacement;
DOI:10.1016/j.tet.2013.02.008
Guidance literature:
Multi-step reaction with 4 steps
1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran; toluene / 21 h / 0 - 20 °C
2.1: sodium hydroxide / tetrahydrofuran; water; methanol / 12 h / 0 - 20 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C
3.2: 21.5 h / 0 - 20 °C
4.1: sodium hydrogencarbonate; methyl iodide / acetonitrile; water / 19 h / 20 °C
With di-isopropyl azodicarboxylate; sodium hydride; sodium hydrogencarbonate; triphenylphosphine; sodium hydroxide; methyl iodide; In tetrahydrofuran; methanol; water; toluene; acetonitrile; mineral oil; 1.1: |Mitsunobu Displacement;
DOI:10.1016/j.tet.2013.02.008
upstream raw materials:

C15H20O3S2

C16H24O3S2

C16H24O3S2

C23H30O3S2

Downstream raw materials:

C43H56O7

C49H70O7Si

C42H54O9

C28H40O8

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