1,12-di-O-acetyl-2,3,4,6,7,8,9,10,11-nona-O-benzyl-L-threo-L-manno-D-gluco-dodeca-1,5-pyranose

Base Information

• Chemical Name: 1,12-di-O-acetyl-2,3,4,6,7,8,9,10,11-nona-O-benzyl-L-threo-L-manno-D-gluco-dodeca-1,5-pyranose
• CAS No.: 1430815-03-4
• Molecular Formula: C₇₉H₈₂O₁₄
• Molecular Weight: 1255.51

Synonyms:1,12-di-O-acetyl-2,3,4,6,7,8,9,10,11-nona-O-benzyl-L-threo-L-manno-D-gluco-dodeca-1,5-pyranose

Chemical Property of 1,12-di-O-acetyl-2,3,4,6,7,8,9,10,11-nona-O-benzyl-L-threo-L-manno-D-gluco-dodeca-1,5-pyranose

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Technology Process of 1,12-di-O-acetyl-2,3,4,6,7,8,9,10,11-nona-O-benzyl-L-threo-L-manno-D-gluco-dodeca-1,5-pyranose

There total 1 articles about 1,12-di-O-acetyl-2,3,4,6,7,8,9,10,11-nona-O-benzyl-L-threo-L-manno-D-gluco-dodeca-1,5-pyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2,3,4,6,7,8,9,10,11-nona-O-benzyl-L-threo-L-manno-α-D-gluco-dodeca-1,5-pyranoside → 1,12-di-O-acetyl-2,3,4,6,7,8,9,10,11-nona-O-benzyl-L-threo-L-manno-D-gluco-dodeca-1,5-pyranose (1430815-02-3) + 1,12-di-O-acetyl-2,3,4,6,7,8,9,10,11-nona-O-benzyl-L-threo-L-manno-D-gluco-dodeca-1,5-pyranose (1430815-03-4)

Guidance literature:

With sulfuric acid; acetic anhydride; In ethyl acetate; at 20 ℃; for 72h; Overall yield = 85 %; Overall yield = 1.64 g;

DOI:10.1016/j.tetasy.2013.03.009

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