Technology Process of C22H15N3O4
There total 7 articles about C22H15N3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C23H17N3O4;
With
water; potassium hydroxide;
In
ethanol;
at 20 ℃;
for 8h;
With
hydrogenchloride;
In
water;
pH=2;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h / 20 °C
1.2: 1 h / 0 - 25 °C
2.1: hydrogenchloride / ethanol; water / 3 h / 80 °C
3.1: formic acid / palladium 10% on activated carbon / ethanol / 5 h / Inert atmosphere; Reflux
3.2: 3 h / 25 - 70 °C
4.1: sodium methylate / methanol / 3 h / 60 °C
4.2: 20 °C
5.1: potassium hydroxide; water / ethanol / 8 h / 20 °C
5.2: pH 2
With
hydrogenchloride; formic acid; potassium tert-butylate; water; sodium methylate; potassium hydroxide;
palladium 10% on activated carbon;
In
methanol; ethanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride / ethanol; water / 3 h / 80 °C
2.1: formic acid / palladium 10% on activated carbon / ethanol / 5 h / Inert atmosphere; Reflux
2.2: 3 h / 25 - 70 °C
3.1: sodium methylate / methanol / 3 h / 60 °C
3.2: 20 °C
4.1: potassium hydroxide; water / ethanol / 8 h / 20 °C
4.2: pH 2
With
hydrogenchloride; formic acid; water; sodium methylate; potassium hydroxide;
palladium 10% on activated carbon;
In
methanol; ethanol; water;
