2-(3,5-dichloro-4-((6-chloro-5-isopropylpyridazin-3-yl)thio)phenyl)ethanol

Base Information

Chemical Name:2-(3,5-dichloro-4-((6-chloro-5-isopropylpyridazin-3-yl)thio)phenyl)ethanol
CAS No.:920509-75-7
Molecular Formula:C₁₅H₁₅Cl₃N₂OS
Molecular Weight:377.722
Hs Code.:

Synonyms:2-(3,5-dichloro-4-((6-chloro-5-isopropylpyridazin-3-yl)thio)phenyl)ethanol

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Chemical Property of 2-(3,5-dichloro-4-((6-chloro-5-isopropylpyridazin-3-yl)thio)phenyl)ethanol

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Technology Process of 2-(3,5-dichloro-4-((6-chloro-5-isopropylpyridazin-3-yl)thio)phenyl)ethanol

There total 1 articles about 2-(3,5-dichloro-4-((6-chloro-5-isopropylpyridazin-3-yl)thio)phenyl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 107228-51-3
3,6-dichloro-4-isopropyl-1,2-dihydropyridazine

: 920509-74-6
2-(3,5-dichloro-4-mercaptophenyl)ethanol

: 920509-75-7
2-(3,5-dichloro-4-((6-chloro-5-isopropylpyridazin-3-yl)thio)phenyl)ethanol

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 90 ℃; for 18h;

Reference yield:

: 920509-75-7
2-(3,5-dichloro-4-((6-chloro-5-isopropylpyridazin-3-yl)thio)phenyl)ethanol

: [3,5-dichloro-4-(5-isopropyl-6-oxo-1,6-dihydropyridazin-3-ylsulfanyl)phenyl]acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Jones reagent / acetone / 1 h / -3 - 0 °C / Inert atmosphere

2: acetic acid; sodium acetate / 24 h / 125 °C / Inert atmosphere

With Jones reagent; sodium acetate; acetic acid; In acetone; 1: |Jones Oxidation;
DOI:10.1021/jm4019299

Reference yield:

: 920509-75-7
2-(3,5-dichloro-4-((6-chloro-5-isopropylpyridazin-3-yl)thio)phenyl)ethanol

: [3,5-dichloro-4-(5-isopropyl-6-oxo-1,6-dihydropyridazine-3-sulfinyl)phenyl]acetic acid

: [3,5-dichloro-4-(5-isopropyl-6-oxo-1,6-dihydropyridazine-3-sulfonyl)phenyl]acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: Jones reagent / acetone / 1 h / -3 - 0 °C / Inert atmosphere

2: acetic acid; sodium acetate / 24 h / 125 °C / Inert atmosphere

3: formic acid; dihydrogen peroxide / water / 168 h / 0 - 25 °C

With Jones reagent; formic acid; dihydrogen peroxide; sodium acetate; acetic acid; In water; acetone; 1: |Jones Oxidation;
DOI:10.1021/jm4019299