C₂₆H₃₄O₇

Base Information

Chemical Name:C₂₆H₃₄O₇
CAS No.:1362110-60-8
Molecular Formula:C₂₆H₃₄O₇
Molecular Weight:458.552
Hs Code.:

C<sub>26</sub>H<sub>34</sub>O<sub>7</sub>

Synonyms:C₂₆H₃₄O₇

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Chemical Property of C₂₆H₃₄O₇

Chemical Property:

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Technology Process of C₂₆H₃₄O₇

There total 14 articles about C₂₆H₃₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 1362110-57-3
C₃₂H₃₆O₈S

: 1362110-37-9
C₂₅H₃₂O₆

: 1362110-60-8
C₂₆H₃₄O₇

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 100 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol300390k

Reference yield:

: C₃₉H₅₁ClO₆Si

: 1362110-37-9
C₂₅H₃₂O₆

: 1362110-60-8
C₂₆H₃₄O₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydroxide / methanol; water / 0.33 h / 20 °C

2.1: N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

3.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

4.2: brine

5.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

6.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.1: sodium cyanoborohydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 66 °C / Inert atmosphere

8.1: ammonia / methanol; water / 6 h / 66 °C

8.2: 0 °C / pH 2

9.1: pyridine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

10.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 100 °C / Inert atmosphere

With pyridine; 1H-imidazole; tert.-butylhydroperoxide; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonate)oxovanadium; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; ammonia; iodine; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 5.1: Sharpless epoxidation;
DOI:10.1021/ol300390k

Reference yield:

: C₃₂H₄₈O₅Si

: 1362110-37-9
C₂₅H₃₂O₆

: 1362110-60-8
C₂₆H₃₄O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

2.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

3.2: brine

4.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

5.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

6.1: sodium cyanoborohydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 66 °C / Inert atmosphere

7.1: ammonia / methanol; water / 6 h / 66 °C

7.2: 0 °C / pH 2

8.1: pyridine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

9.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 100 °C / Inert atmosphere

With pyridine; 1H-imidazole; tert.-butylhydroperoxide; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonate)oxovanadium; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; ammonia; iodine; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 4.1: Sharpless epoxidation;
DOI:10.1021/ol300390k