4-azido-3-O-benzyl-4,6-dideoxy-2-O-levulinoyl-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside trichloroacetimidate

Base Information

• Chemical Name: 4-azido-3-O-benzyl-4,6-dideoxy-2-O-levulinoyl-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside trichloroacetimidate
• CAS No.: 1239319-02-8
• Molecular Formula: C₄₀H₄₃Cl₃N₄O₁₁
• Molecular Weight: 862.161

Synonyms:4-azido-3-O-benzyl-4,6-dideoxy-2-O-levulinoyl-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside trichloroacetimidate

Chemical Property of 4-azido-3-O-benzyl-4,6-dideoxy-2-O-levulinoyl-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside trichloroacetimidate

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Technology Process of 4-azido-3-O-benzyl-4,6-dideoxy-2-O-levulinoyl-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside trichloroacetimidate

There total 1 articles about 4-azido-3-O-benzyl-4,6-dideoxy-2-O-levulinoyl-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

C38H43N3O11 + trichloroacetonitrile (545-06-2) → 4-azido-3-O-benzyl-4,6-dideoxy-2-O-levulinoyl-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside trichloroacetimidate (1239319-02-8)

Guidance literature:

With sodium hydride; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/ja104027w

Reference yield: 82.0%

pent-4-enyl 2-O-benzoyl-4-O-benzyl-α-L-rhamnosyl-(1->3)-3,4-di-O-benzyl-α-L-rhamnoside (1239319-01-7) + 4-azido-3-O-benzyl-4,6-dideoxy-2-O-levulinoyl-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside trichloroacetimidate (1239319-02-8) → pent-4-enyl 4-azido-3-O-benzyl-4,6-dideoxy-2-O-levulinoyl-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside (1239319-03-9)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃;

DOI:10.1021/ja104027w

upstream raw materials:

trichloroacetonitrile

Downstream raw materials:

pent-4-enyl 4-azido-3-O-benzyl-4,6-dideoxy-2-O-levulinoyl-β-D-glucopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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