allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3[2-O-benzyl-6-O-(4-methoxy)benzyl]-β-D-glucopyranoside

Base Information

• Chemical Name: allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3[2-O-benzyl-6-O-(4-methoxy)benzyl]-β-D-glucopyranoside
• CAS No.: 200003-53-8
• Molecular Formula: C₅₁H₅₈O₁₁
• Molecular Weight: 847.015

Synonyms:allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3[2-O-benzyl-6-O-(4-methoxy)benzyl]-β-D-glucopyranoside

Chemical Property of allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3[2-O-benzyl-6-O-(4-methoxy)benzyl]-β-D-glucopyranoside

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Technology Process of allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3[2-O-benzyl-6-O-(4-methoxy)benzyl]-β-D-glucopyranoside

There total 1 articles about allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3[2-O-benzyl-6-O-(4-methoxy)benzyl]-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3[2-O-benzyl-4,6-O-(4-methoxy)benzylidene]-β-D-glucopyranoside (200003-37-8) → allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3(2-O-benzyl)-β-D-glucopyranoside (200003-54-9) + allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3[2-O-benzyl-4-O-(4-methoxy)benzyl]-β-D-glucopyranoside + allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3[2-O-benzyl-6-O-(4-methoxy)benzyl]-β-D-glucopyranoside (200003-53-8)

Guidance literature:

With aluminium trichloride; 4 A molecular sieve; trimethylamine borane; In tetrahydrofuran; at 0 - 20 ℃; for 4.2h;

DOI:10.1016/S0040-4020(97)01024-7

Reference yield: 96.0%

2,3,4-tri-O-acetyl-6-O-benzyl-α,β-D-galactopyranosyl trichloroacetimidate (169393-72-0) + allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3[2-O-benzyl-6-O-(4-methoxy)benzyl]-β-D-glucopyranoside (200003-53-8) → acetic acid 4,5-diacetoxy-2-[6-allyloxy-5-benzyloxy-2-(4-methoxy-benzyloxymethyl)-4-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yloxy]-6-benzyloxymethyl-tetrahydro-pyran-3-yl ester

Guidance literature:

With trifluorormethanesulfonic acid; In diethyl ether; at 0 ℃;

DOI:10.1016/S0040-4020(97)01024-7

Reference yield: 95.0%

2,3,4,6-tetra-O-acetyl-D-galactopyranosyl trichloroacetimidate (74808-10-9,86520-63-0,87119-53-7,92052-29-4,121238-27-5,142831-80-9,127061-80-7) + allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3[2-O-benzyl-6-O-(4-methoxy)benzyl]-β-D-glucopyranoside (200003-53-8) → acetic acid 4,5-diacetoxy-6-acetoxymethyl-2-[6-allyloxy-5-benzyloxy-2-(4-methoxy-benzyloxymethyl)-4-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yloxy]-tetrahydro-pyran-3-yl ester

Guidance literature:

With trifluorormethanesulfonic acid; In diethyl ether; at 0 ℃;

DOI:10.1016/S0040-4020(97)01024-7

upstream raw materials:

allyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)1->3[2-O-benzyl-4,6-O-(4-methoxy)benzylidene]-β-D-glucopyranoside

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