(1S,3S)-trans-3-tert-butylcyclohexanol

Base Information

Chemical Name:(1S,3S)-trans-3-tert-butylcyclohexanol
CAS No.:69854-68-8
Molecular Formula:C₁₀H₂₀O
Molecular Weight:156.268
Hs Code.:

Synonyms:(1S,3S)-trans-3-tert-butylcyclohexanol

Suppliers and Price of (1S,3S)-trans-3-tert-butylcyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,3S)-trans-3-tert-butylcyclohexanol

Chemical Property:

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Technology Process of (1S,3S)-trans-3-tert-butylcyclohexanol

There total 11 articles about (1S,3S)-trans-3-tert-butylcyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 936-99-2
3-tert-butylcyclohexanone

: 69854-68-8
(1S,3S)-trans-3-tert-butylcyclohexanol

Guidance literature:: With NAD⁺-HLAD; In ethanol; for 1008h; Yield given;

Reference yield:

: 936-99-2
3-tert-butylcyclohexanone

: 61116-78-7
(1S,3R)-3-tert-butyl-cyclohexanol

: 69854-68-8
(1S,3S)-trans-3-tert-butylcyclohexanol

Guidance literature:: With C₁₂H₂₁N₅⁽²⁺⁾*2Cl^(1-); potassium tert-butylate; hydrogen; cobalt(II) chloride; In tetrahydrofuran; at 60 ℃; for 16h; under 37503.8 Torr; Overall yield = 90 %; stereoselective reaction; Autoclave;
DOI:10.1016/j.chempr.2019.03.010

Reference yield:

: 585-34-2
3-tert-butylphenyol

: 4534-70-7,10488-10-5,13492-08-5,13492-09-6,16201-66-4,61116-78-7,61116-79-8,69854-68-8,77286-43-2
trans-(1R,3S)-tert-butylcyclohexanol

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / H₂ / 5percent Rh/C / methanol

2: 89 percent / CrO₃-H₂SO₄ / acetone

3: 1.) LiAlH₄, 2.) pyridine / 1.) Et₂O

4: 1.) brucine / 2.) saponification

With pyridine; chromium(VI) oxide; lithium aluminium tetrahydride; sulfuric acid; hydrogen; brucine; Rh on carbon; In methanol; acetone;
DOI:10.1021/ja00408a007