Ph₃GeGeBu(n)2GeBu(n)2CH₂CH₂OEt

Base Information

Chemical Name:Ph₃GeGeBu(n)2GeBu(n)2CH₂CH₂OEt
CAS No.:894804-44-5
Molecular Formula:C₃₈H₆₀Ge₃O
Molecular Weight:750.664
Hs Code.:

Ph<sub>3</sub>GeGeBu(n)2GeBu(n)2CH<sub>2</sub>CH<sub>2</sub>OEt

Synonyms:Ph₃GeGeBu(n)2GeBu(n)2CH₂CH₂OEt

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Chemical Property of Ph₃GeGeBu(n)2GeBu(n)2CH₂CH₂OEt

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Technology Process of Ph₃GeGeBu(n)2GeBu(n)2CH₂CH₂OEt

There total 1 articles about Ph₃GeGeBu(n)2GeBu(n)2CH₂CH₂OEt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 894804-36-5
Bu₂Ge(NMe₂)CH₂CH₂OEt

: 894804-43-4
Ph₃GeGe(Bu)2H

: 894804-44-5
Ph₃GeGeBu(n)2GeBu(n)2CH₂CH₂OEt

Guidance literature:: In acetonitrile; High Pressure; under inert atm. to soln. Ph3GeGe(Bu)2H in MeCN soln. Bu2Ge(NMe2)CH2CH2OEt in MeCN was added and heated in tube sealed with Teflon plug at 85°C for 48 h; volatiles were removed in vacuo, residue was distilled in Kugelrohr oven(100°C, 0.08 Torr) for 3 h; elem. anal.;
DOI:10.1021/om060115x

Reference yield: 75.0%

: 894804-36-5
Bu₂Ge(NMe₂)CH₂CH₂OEt

: 894804-44-5
Ph₃GeGeBu(n)2GeBu(n)2CH₂CH₂OEt

: 894804-46-7
Ph₃GeGe(Bu)2Ge(Bu)2Ge(Bu)2CH₂CH₂OEt

Guidance literature:: With DIBAL-H; In acetonitrile; High Pressure; under N2 atm. to soln. Ph3GeGe(Bu)2Ge(Bu)2CH2CH2OEt in benzene was addedsoln. DIBAL-H in hexane, refluxed for 24 h, soln. was allowed to cool, volatiles were removed in vacuo, soln. Bu2Ge(NMe2)CH2CH2OEt in MeCN was added, heated at 95°C for 48 h; volatiles were removed in vacuo, residue was filtered through silica column (benzene), solvent was removed; identified by NMR;
DOI:10.1021/om060115x

Reference yield:

: 894804-44-5
Ph₃GeGeBu(n)2GeBu(n)2CH₂CH₂OEt

: 894804-46-7
Ph₃GeGe(Bu)2Ge(Bu)2Ge(Bu)2CH₂CH₂OEt

Guidance literature:: Multi-step reaction with 2 steps

1: benzene; hexane

2: acetonitrile

In hexane; acetonitrile; benzene;
DOI:10.1021/om060115x