dibenzyl 2-((tert-butoxycarbonyl)amino)-6-(5-oxo-5-(undecyloxy)pentanamido)heptanedioate

Base Information

Chemical Name:dibenzyl 2-((tert-butoxycarbonyl)amino)-6-(5-oxo-5-(undecyloxy)pentanamido)heptanedioate
CAS No.:1269619-97-7
Molecular Formula:C₄₂H₆₂N₂O₉
Molecular Weight:738.962
Hs Code.:

Synonyms:dibenzyl 2-((tert-butoxycarbonyl)amino)-6-(5-oxo-5-(undecyloxy)pentanamido)heptanedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzyl 2-((tert-butoxycarbonyl)amino)-6-(5-oxo-5-(undecyloxy)pentanamido)heptanedioate

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Technology Process of dibenzyl 2-((tert-butoxycarbonyl)amino)-6-(5-oxo-5-(undecyloxy)pentanamido)heptanedioate

There total 8 articles about dibenzyl 2-((tert-butoxycarbonyl)amino)-6-(5-oxo-5-(undecyloxy)pentanamido)heptanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 112-42-5
undecyl alcohol

: 1269619-96-6
5-((1,7-bis(benzyloxy)-6-(-(tert-butoxycarbonyl)amino)-1,7-dioxoheptan-2-yl)amino)-5-oxopentanoic acid

: 1269619-97-7
dibenzyl 2-((tert-butoxycarbonyl)amino)-6-(5-oxo-5-(undecyloxy)pentanamido)heptanedioate

Guidance literature:: With dmap; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1021/jm101535e

Reference yield:

: 108-55-4
glutaric anhydride,

: 1269619-97-7
dibenzyl 2-((tert-butoxycarbonyl)amino)-6-(5-oxo-5-(undecyloxy)pentanamido)heptanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 1 h / 20 °C

2: dmap; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 12 h / 20 °C

With dmap; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm101535e

Reference yield:

: 1227363-56-5
dibenzyl 2,6-bis((tert-butoxycarbonyl)amino)heptanedioate

: 1269619-97-7
dibenzyl 2-((tert-butoxycarbonyl)amino)-6-(5-oxo-5-(undecyloxy)pentanamido)heptanedioate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / 1,4-dioxane / 2 h

2: triethylamine / methanol / 0.5 h / pH 7

3: dichloromethane / 1 h / 20 °C

4: dmap; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 12 h / 20 °C

With hydrogenchloride; dmap; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm101535e