N-((2S,3S,6R)-6-allyl-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide

Base Information

Chemical Name:N-((2S,3S,6R)-6-allyl-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide
CAS No.:1101117-87-6
Molecular Formula:C₃₀H₂₈Cl₃NO₃
Molecular Weight:556.916
Hs Code.:

Synonyms:N-((2S,3S,6R)-6-allyl-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide

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Chemical Property of N-((2S,3S,6R)-6-allyl-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide

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Technology Process of N-((2S,3S,6R)-6-allyl-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide

There total 1 articles about N-((2S,3S,6R)-6-allyl-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1101117-86-5
(2R,3R,6S)-2-allyl-6-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl 2,2,2-trichloroacetimidate

: 1101117-87-6
N-((2S,3S,6R)-6-allyl-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide

Guidance literature:: With potassium carbonate; In 5,5-dimethyl-1,3-cyclohexadiene; at 150 ℃; for 12h;
DOI:10.1039/b810654a

Reference yield: 62.0%

: 1101117-87-6
N-((2S,3S,6R)-6-allyl-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide

: 1101117-89-8
C₃₀H₃₀Cl₃NO₅

Guidance literature:: N-((2S,3S,6R)-6-allyl-2-(trityloxymethyl)-3,6-dihydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide; With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; tert-butyl alcohol; at 20 ℃; for 3h;

With sodium disulfite; In water; acetone; tert-butyl alcohol; for 0.166667h; regioselective reaction;
DOI:10.1039/b810654a