1-[2-O-acetyl-3-deoxy-3-carboxymethyl-5-O-(p-methoxytrityl)-pentofuranosyl]-uracil

Base Information

Chemical Name:1-[2-O-acetyl-3-deoxy-3-carboxymethyl-5-O-(p-methoxytrityl)-pentofuranosyl]-uracil
CAS No.:1287721-51-0
Molecular Formula:C₃₃H₃₂N₂O₈
Molecular Weight:584.626
Hs Code.:

Synonyms:1-[2-O-acetyl-3-deoxy-3-carboxymethyl-5-O-(p-methoxytrityl)-pentofuranosyl]-uracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[2-O-acetyl-3-deoxy-3-carboxymethyl-5-O-(p-methoxytrityl)-pentofuranosyl]-uracil

Chemical Property:

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Technology Process of 1-[2-O-acetyl-3-deoxy-3-carboxymethyl-5-O-(p-methoxytrityl)-pentofuranosyl]-uracil

There total 4 articles about 1-[2-O-acetyl-3-deoxy-3-carboxymethyl-5-O-(p-methoxytrityl)-pentofuranosyl]-uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₄H₃₆N₂O₉

: 1287721-51-0
1-[2-O-acetyl-3-deoxy-3-carboxymethyl-5-O-(p-methoxytrityl)-pentofuranosyl]-uracil

Guidance literature:: With sodium periodate; In 1,4-dioxane; water; at 20 ℃; for 10h; Inert atmosphere;
DOI:10.1002/anie.201007012

Reference yield:

: 1022902-92-6
1-[3-allyl-3-deoxy-pentofuranosyl]-uracil

: 1287721-51-0
1-[2-O-acetyl-3-deoxy-3-carboxymethyl-5-O-(p-methoxytrityl)-pentofuranosyl]-uracil

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 0 - 20 °C / Inert atmosphere

2: pyridine; dmap / 4 h / 20 °C / Inert atmosphere

3: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / 1,4-dioxane / 10 h / 20 °C / Inert atmosphere

4: sodium periodate / 1,4-dioxane; water / 10 h / 20 °C / Inert atmosphere

With pyridine; dmap; sodium periodate; osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In 1,4-dioxane; water;
DOI:10.1002/anie.201007012

Reference yield:

: 200011-14-9
1-[3-C-allyl-2,5-O-bis(tert-butyldimethylsilyl)-β-D-pentofuranosyl]-uracyl

: 1287721-51-0
1-[2-O-acetyl-3-deoxy-3-carboxymethyl-5-O-(p-methoxytrityl)-pentofuranosyl]-uracil

Guidance literature:: Multi-step reaction with 5 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

2: pyridine / 0 - 20 °C / Inert atmosphere

3: pyridine; dmap / 4 h / 20 °C / Inert atmosphere

4: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / 1,4-dioxane / 10 h / 20 °C / Inert atmosphere

5: sodium periodate / 1,4-dioxane; water / 10 h / 20 °C / Inert atmosphere

With pyridine; dmap; sodium periodate; osmium(VIII) oxide; tetrabutyl ammonium fluoride; water; 4-methylmorpholine N-oxide; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1002/anie.201007012