3-(2,4,6-triisopropylphenyl)-3-{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-5,5-diphenyl-1,2,4,3-triselenastannolane

Base Information

Chemical Name:3-(2,4,6-triisopropylphenyl)-3-{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-5,5-diphenyl-1,2,4,3-triselenastannolane
CAS No.:144602-86-8
Molecular Formula:C₅₅H₉₂Se₃Si₆Sn
Molecular Weight:1277.44
Hs Code.:

Synonyms:3-(2,4,6-triisopropylphenyl)-3-{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-5,5-diphenyl-1,2,4,3-triselenastannolane

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Chemical Property of 3-(2,4,6-triisopropylphenyl)-3-{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-5,5-diphenyl-1,2,4,3-triselenastannolane

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Technology Process of 3-(2,4,6-triisopropylphenyl)-3-{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-5,5-diphenyl-1,2,4,3-triselenastannolane

There total 3 articles about 3-(2,4,6-triisopropylphenyl)-3-{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-5,5-diphenyl-1,2,4,3-triselenastannolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 138423-63-9
5-(2,4,6-triisopropylphenyl)-5-{2,4,6-tris{bis(trimethylsilyl)methyl}phenyl}-1,2,3,4,5-tetraselenastannolane

: 908093-98-1
diazodiphenylmethane

: 144602-85-7
3-(2,4,6-triisopropylphenyl)-3-{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-6,6-diphenyl-1,2,4,5-tetraselena-3-stannacyclohexane

: 144602-86-8
3-(2,4,6-triisopropylphenyl)-3-{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-5,5-diphenyl-1,2,4,3-triselenastannolane

Guidance literature:: In benzene; refluxed for 10 h under Ar; evapd., chromy., recrystn. (ethanol/CHCl3), elem. anal.;
DOI:10.1021/om00031a030

Reference yield: 63.0%

: 144602-85-7
3-(2,4,6-triisopropylphenyl)-3-{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-6,6-diphenyl-1,2,4,5-tetraselena-3-stannacyclohexane

: 144602-86-8
3-(2,4,6-triisopropylphenyl)-3-{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-5,5-diphenyl-1,2,4,3-triselenastannolane

Guidance literature:: With HMPT; In tetrahydrofuran; addn. of HMPT to the stannacyclohexane in THF at room temp., stirred for 10 h under Ar; evapd., chromy.;
DOI:10.1021/om00031a030

Reference yield:

: 138423-63-9
5-(2,4,6-triisopropylphenyl)-5-{2,4,6-tris{bis(trimethylsilyl)methyl}phenyl}-1,2,3,4,5-tetraselenastannolane

: 908093-98-1
diazodiphenylmethane

: 144602-86-8
3-(2,4,6-triisopropylphenyl)-3-{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-5,5-diphenyl-1,2,4,3-triselenastannolane

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: HMPT / tetrahydrofuran

With HMPT; In tetrahydrofuran; benzene;
DOI:10.1021/om00031a030