Technology Process of C20H26N4O3S
There total 5 articles about C20H26N4O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H24N2O4S;
With
water; lithium hydroxide;
In
methanol;
for 3h;
aniline;
With
diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: chloroform / 20 °C
2.1: tetraphosphorus decasulfide; sodium carbonate / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere
3.1: N-Bromosuccinimide / 1,4-dioxane; water / 0 - 20 °C
3.2: 1 h / 100 °C
4.1: water; lithium hydroxide / methanol / 3 h
4.2: 12 h / 100 °C
With
N-Bromosuccinimide; tetraphosphorus decasulfide; water; sodium carbonate; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; chloroform; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: chloroform / 20 °C
2.1: tetraphosphorus decasulfide; sodium carbonate / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere
3.1: N-Bromosuccinimide / 1,4-dioxane; water / 0 - 20 °C
3.2: 1 h / 100 °C
4.1: water; lithium hydroxide / methanol / 3 h
4.2: 12 h / 100 °C
With
N-Bromosuccinimide; tetraphosphorus decasulfide; water; sodium carbonate; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; chloroform; water;