(1S,4aR,7R,7aS)-1-(N-methyl-N-phenyl)amino-4,7-dimethyl-2-oxa-1,2,4a,7a-tetrahydroindane

Base Information

Chemical Name:(1S,4aR,7R,7aS)-1-(N-methyl-N-phenyl)amino-4,7-dimethyl-2-oxa-1,2,4a,7a-tetrahydroindane
CAS No.:105582-23-8
Molecular Formula:C₁₇H₂₃NO
Molecular Weight:257.376
Hs Code.:

Synonyms:(1S,4aR,7R,7aS)-1-(N-methyl-N-phenyl)amino-4,7-dimethyl-2-oxa-1,2,4a,7a-tetrahydroindane

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Chemical Property of (1S,4aR,7R,7aS)-1-(N-methyl-N-phenyl)amino-4,7-dimethyl-2-oxa-1,2,4a,7a-tetrahydroindane

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Technology Process of (1S,4aR,7R,7aS)-1-(N-methyl-N-phenyl)amino-4,7-dimethyl-2-oxa-1,2,4a,7a-tetrahydroindane

There total 3 articles about (1S,4aR,7R,7aS)-1-(N-methyl-N-phenyl)amino-4,7-dimethyl-2-oxa-1,2,4a,7a-tetrahydroindane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73127-93-2
(R)-3,7-dimethyl-6(E)-octene-1,8-diol

: 100-61-8
N-methylaniline

: 105582-23-8
(1S,4aR,7R,7aS)-1-(N-methyl-N-phenyl)amino-4,7-dimethyl-2-oxa-1,2,4a,7a-tetrahydroindane

Guidance literature:: With 4 A molecular sieve; In diethyl ether; for 10h; Yield given; Ambient temperature;
DOI:10.1021/ja00286a034

Reference yield:

: 2385-77-5
(R)-Citronellal

: 105582-23-8
(1S,4aR,7R,7aS)-1-(N-methyl-N-phenyl)amino-4,7-dimethyl-2-oxa-1,2,4a,7a-tetrahydroindane

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / SeO₂, tBuOOH

2: 4A molecular sieve / diethyl ether / 10 h / Ambient temperature

With tert.-butylhydroperoxide; selenium(IV) oxide; 4 A molecular sieve; In diethyl ether;
DOI:10.1021/ja00286a034

Reference yield:

: 2385-77-5
(R)-Citronellal

: 105582-23-8
(1S,4aR,7R,7aS)-1-(N-methyl-N-phenyl)amino-4,7-dimethyl-2-oxa-1,2,4a,7a-tetrahydroindane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) selenium dioxide, t-butyl hydroperoxide / 1.) toluene, 0-5 deg C, 30 min, 2.) toluene, 20-25 deg C

2: MS 4A / diethyl ether / 16 h / Ambient temperature

With tert.-butylhydroperoxide; selenium(IV) oxide; In diethyl ether;