Technology Process of (1S,4aR,7R,7aS)-1-(N-methyl-N-phenyl)amino-4,7-dimethyl-2-oxa-1,2,4a,7a-tetrahydroindane
There total 3 articles about (1S,4aR,7R,7aS)-1-(N-methyl-N-phenyl)amino-4,7-dimethyl-2-oxa-1,2,4a,7a-tetrahydroindane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
4 A molecular sieve;
In
diethyl ether;
for 10h;
Yield given;
Ambient temperature;
DOI:10.1021/ja00286a034
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 45 percent / SeO2, tBuOOH
2: 4A molecular sieve / diethyl ether / 10 h / Ambient temperature
With
tert.-butylhydroperoxide; selenium(IV) oxide; 4 A molecular sieve;
In
diethyl ether;
DOI:10.1021/ja00286a034
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) selenium dioxide, t-butyl hydroperoxide / 1.) toluene, 0-5 deg C, 30 min, 2.) toluene, 20-25 deg C
2: MS 4A / diethyl ether / 16 h / Ambient temperature
With
tert.-butylhydroperoxide; selenium(IV) oxide;
In
diethyl ether;
