(1,2,4)Triazino(3,4-f)purine-7(4H)-acetic acid, 1-ethyl-1,6,8,9-tetrahydro-9-methyl-6,8-dioxo-3-phenyl-, hydrazide

Base Information

Chemical Name:(1,2,4)Triazino(3,4-f)purine-7(4H)-acetic acid, 1-ethyl-1,6,8,9-tetrahydro-9-methyl-6,8-dioxo-3-phenyl-, hydrazide
CAS No.:105774-59-2
Molecular Formula:C18H20 N8 O3
Molecular Weight:396.4032
Hs Code.:
DSSTox Substance ID:DTXSID50147333

Synonyms:BRN 5671896;105774-59-2;(1,2,4)Triazino(3,4-f)purine-7(4H)-acetic acid, 1-ethyl-1,6,8,9-tetrahydro-9-methyl-6,8-dioxo-3-phenyl-, hydrazide;DTXSID50147333;LS-155709

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1,2,4)Triazino(3,4-f)purine-7(4H)-acetic acid, 1-ethyl-1,6,8,9-tetrahydro-9-methyl-6,8-dioxo-3-phenyl-, hydrazide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：136.03000
Density:1.57g/cm³
LogP:0.17200
XLogP3:0.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:4
Exact Mass:396.16583653
Heavy Atom Count:29
Complexity:722

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN1C2=NC3=C(N2CC(=N1)C4=CC=CC=C4)C(=O)N(C(=O)N3C)CC(=O)NN

Technology Process of (1,2,4)Triazino(3,4-f)purine-7(4H)-acetic acid, 1-ethyl-1,6,8,9-tetrahydro-9-methyl-6,8-dioxo-3-phenyl-, hydrazide

There total 2 articles about (1,2,4)Triazino(3,4-f)purine-7(4H)-acetic acid, 1-ethyl-1,6,8,9-tetrahydro-9-methyl-6,8-dioxo-3-phenyl-, hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 105774-55-8
(1-Ethyl-8-methyl-5,7-dioxo-3-phenyl-1,5,7,8-tetrahydro-4H-1,2,4a,6,8,9-hexaaza-fluoren-6-yl)-acetic acid ethyl ester

: 105774-59-2
(1-Ethyl-8-methyl-5,7-dioxo-3-phenyl-1,5,7,8-tetrahydro-4H-1,2,4a,6,8,9-hexaaza-fluoren-6-yl)-acetic acid hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 0.5h; Heating;
DOI:10.1007/BF00758812

Reference yield:

: 81147-04-8
1-Ethyl-8-methyl-3-phenyl-1,4-dihydro-8H-1,2,4a,6,8,9-hexaaza-fluorene-5,7-dione

: 105774-59-2
(1-Ethyl-8-methyl-5,7-dioxo-3-phenyl-1,5,7,8-tetrahydro-4H-1,2,4a,6,8,9-hexaaza-fluoren-6-yl)-acetic acid hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / K₂CO₃ / dimethylformamide / 2 h / Heating

2: 77 percent / hydrazine hydrate / ethanol / 0.5 h / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1007/BF00758812