C₄₂H₅₆O₄Si

Base Information

Chemical Name:C₄₂H₅₆O₄Si
CAS No.:1453486-50-4
Molecular Formula:C₄₂H₅₆O₄Si
Molecular Weight:652.99
Hs Code.:

C<sub>42</sub>H<sub>56</sub>O<sub>4</sub>Si

Synonyms:C₄₂H₅₆O₄Si

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Chemical Property of C₄₂H₅₆O₄Si

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Technology Process of C₄₂H₅₆O₄Si

There total 17 articles about C₄₂H₅₆O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1453486-49-1
C₄₂H₅₈O₄Si

: 1453486-50-4
C₄₂H₅₆O₄Si

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetasy.2013.07.002

Reference yield:

: 1453486-44-6
ethyl (R,2Z,5Z,9E)-12-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-11-hydroxy-3,6-dimethyldodeca-2,5,9-trienoate

: 1453486-50-4
C₄₂H₅₆O₄Si

Guidance literature:: Multi-step reaction with 6 steps

1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: (R)-10-camphorsulfonic acid / methanol / 4 h / 20 °C / Inert atmosphere

3: pyridine / dichloromethane / 4 h / 0 °C / Inert atmosphere

4: 1H-imidazole / dichloromethane / 5 h / 20 °C / Inert atmosphere

5: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -15 °C / Inert atmosphere

6: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

With pyridine; 1H-imidazole; (R)-10-camphorsulfonic acid; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; In methanol; dichloromethane; toluene; 6: |Dess-Martin Oxidation;
DOI:10.1016/j.tetasy.2013.07.002

Reference yield:

: 1453486-45-7
ethyl (R,2Z,5Z,9E)-12-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-11-methoxy-3,6-dimethyldodeca-2,5,9-trienoate

: 1453486-50-4
C₄₂H₅₆O₄Si

Guidance literature:: Multi-step reaction with 5 steps

1: (R)-10-camphorsulfonic acid / methanol / 4 h / 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 4 h / 0 °C / Inert atmosphere

3: 1H-imidazole / dichloromethane / 5 h / 20 °C / Inert atmosphere

4: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -15 °C / Inert atmosphere

5: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

With pyridine; 1H-imidazole; (R)-10-camphorsulfonic acid; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; In methanol; dichloromethane; toluene; 5: |Dess-Martin Oxidation;
DOI:10.1016/j.tetasy.2013.07.002